GCMS Sample AE03436 Report, March 12 2002

Machine-extracted title · confidence 95%

Initial GCMS analysis report for sample AE03436 conducted by analyst DLV on March 12, 2002.

NYC-WTC_000006337–000006347

Folder label: “GCMS X 2/14/02 A 2/23/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB2102\3436.D Vial: 56 Acq On : 23 Feb 2002 11:16 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

8.35 0.34 ug/1 23778 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 9 2 2-Acetyl-l, 4,5,6-tetrahydropyridine 125 C7H11NO 000000-00-0 4 3 2H-Azepin-2-one) hexahydro-5-methyl 127 C7H13NO 002210-07-3 3 4 Formic acid, ethyl ester 74 C3H602 000109-94-4 3 Abundance Scan 361 (8.354 min): 3436 D (-) i m/ z 42.95100.00% 43

5000

97 125 1 ' I ' ' ' 'I 14T 1 I ' 1073 1 1

m/Z-> 10 ■ • । > ..................... T1ZEITTIBITTBT 35 1 49 ... 74.13 II 1 ‘ I 1 ' ' 1 I ' ' 1 ' I ' ' 1 1 I ' ’ 1 • i■ ■ ■ • i ■■ ■ ■ i • ■■ « । ■ ‘ 4 ।■ ■ 8.00 m/ z 8.20 8.40 8.60_____ 46.95 19.47% 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1.1,1-trichlora- 43

5000 _ 8 00 8.20 8.40 8.60_______ 15 m/z 96.95 16.82%| | 35 | ,49 85 97 117 125 1 1 | 1 1 1 1 | 1 ' ' ' | ‘ 1 | ‘ < I I | 1 ' I > | I ' < ' | ) I ! ' | I I'> ! | I I I'I‘| ‘ | । 1 । | । । I I | ! I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 43 54 82 8.00 8.20 8.40 8.60_____ 5000 125 m/z 124.85 16.58%

97 110 ‘I" 1 ■ । 1 ■r ‘ । ■ ■ ■11 ‘ ‘1 111 ■ ‘ । 11 ■11 ■1 1 ■ ।1 ■1 ■ । ■ ■ ■r ।' ■ 1 ■ । ■111 '' ■ । ■1 m/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4753: 2H-Azepin-2-one, hexahydro-5-methyl- i 1 I ■ ■ ' ■ i ' ! 30 8.00 8.20 8.40 8.60_______ m/z 82.85 13.62% J 5000 55 69 99 42 110 127 ' 34 । 111'1 1 । * ■ ■ ■ i 1 1 । । । < i ' > । > । । I Lr11 r ! I 1 - ' i ' ' ' ' i ' ' ' ■ i ■ ' ■ i m1/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 8.00 8.20 8.40 8.60

3436.D GCMS0208.M Fri Mar 08 09:49:50 2002 Page 3

NYC-WTC_000006346

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