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GCMS analysis results for sample AE01330, Feb 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AE01330 conducted on February 27, 2002.

NYC-WTC_000052868–000052874

Folder label: “GCMS X 1/10/02 A 2/19/02

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Ave or Public Portal Document 909 tor*- —..A 709 GALVS quantitation Report (QT Reviewed)

ata File : C:\HPCHEM\1\DATA\FEB1902\1330.D Vial: 15 cq On : 19 Feb 2002 11:59 pm Operator: 209 GALOS •ample : gc/ms scan 1/18 Inst : GC/MS 209 isc : Multiplr: 1.00 3 Integration Params: GOOFY.P ant Time: Feb 21 15:16 2002 (Quant Results File: GCMSO208.RES

ant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) tie : 209 625/TCLP calibration table st Update : Wed Feb 13 11:43:23 2002 ponse via : Initial Calibration aAcq Meth : GCMS0208

al Standards R.T. Qlon Response Cone Units Dev(Min)

.,4-Dichlorobenzene-d4 12.33 152 243307 20.00 ug/1 -0.02 aphthalene-d8 15.98 136 920843 20.00 ug/1 -0.02 cenaphthene-dlO 21.28 164 477291 20.00 ug/1 -0.03 enanthrene-d10 25.74 188 647424 20.00 ug/1 -0.03 irysene-dl2 33.80 240 395092 20.00 ug/1 -0.05 rylene-d12 38.07 264 248947 20.00 ug/1 -0.05

Monitoring Compounds 4-DDD 30.81 235 23011 3.54 ug/mL 0.31 i Amount 5.000 Recovery = 70.80%

'ompounds Qvalue itroso-dimethyl amine 0.00 74 0 N.D. (2-Chloroethyl)ether 0.00 93 0 N.D. -Dichlorobenzene 0.00 146 0 N.D. Dichlorobenzene 0.00 146 0 N.D. Dichlorobenzene 0.00 146 0 N.D. -oxybis{l-Chloropropan 0.00 45 0 N.D. -roso-di -n-propylamine 0.00 70 0 N.D. hloroethane 0.00 117 0 N.D. >benzene 0.00 77 0 N.D. orone 0.00 82 0 N.D. -Chloroethoxy)methane 0.00 93 0 N.D. -Trichlorobenzene 0.00 180 0 N.D. lalene 16.03 128 338 N.D. lorobutadiene 0.00 225 0 N.D. lorocyclopentadiene 0.00 237 0 N.D. ronaphthalene 0.00 162 0 N.D. /lphthalate 0.00 163 0 N.D. litrotoluene 0.00 165 0 N.D. thylene 0.00 152 0 N.D. thene 0.00 153 0 N.D. itrotoluene 0.00 165 0 N.D. phthalate 22.76 149 337 N.D. page 2 phenyl-phenylether 0.00 204 0 N.D. 0.00 166 0 N.D. n/ 1,2-Diphenylhyd 0.00 77 0 N.D.

r out of range (m) = manual integration '08.M Thu Feb 21 15:17:27 2002 Page 1

NYC-WTC_00005287°

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NYC-WTC_000052870Source: NYC Law Department, mirrored locally

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