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GCMS analysis results for sample AE01330, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AE01330 conducted on February 27, 2002.

NYC-WTC_000052868–000052874

Folder label: “GCMS X 1/10/02 A 2/19/02

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Scanned page image, NYC-WTC_000052871
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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1902\1330.D Vial: 15 . Acq On : 19 Feb 2002 11:59 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 12.332 789 794 804 rVB 564171 1346416 71.09% 15.050% 2 15.967 1185 1190 1204 rVB 833860 1765842 93.24% 19.73.9% 3 21.283 1763 1769 1778 rBV 919746 1893959 100.00% 21.171% 4 25.735 2248 2254 2266 rBV2 811195 1728812 91.28% 19.325% 5 30.812 2802 2807 2812 rBV 62265 115697 6.11% 1.293%

6 33.796 3126 3132 3146 rBV2 531267 1199511 63.33% 13.408% 7 38.074 3590 3598 3611 rBV2 297998 873241 46.11% 9.761% 8 45.519 4408 4409 4411 rBV 38954 22594 1.19% 0.253%

Sum of corrected areas: 8946072

1330.D GCMS0208.M Thu Feb 21 15:25:10 2002

NYC-WTC_000052871

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NYC-WTC_000052871Source: NYC Law Department, mirrored locally

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