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GCMS analysis report for sample AE01225, Feb 2002

Machine-extracted title · confidence 50%

GC/MS analysis report for sample AE01225 showing surrogate recovery data generated on February 25, 2002.

NYC-WTC_000052815–000052823

Folder label: “GCMS X 1/17/02 A 2/16/02

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Scanned page image, NYC-WTC_000052820
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1502\1225.D Vial: 27 . Acq On : 16 Feb 2002 6:36 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.208 340 345 350 rBV 10795 23647 1.04% 0.213% 2 12.330 789 794 809 rVB 778302 1694830 74.78% 15.286% 3 15.975 1185 1191 1207 rBV 1048564 2058916 90.84% 18.570% 4 21.290 1763 1770 1785 rBV 1101001 2266458 100.00% 20.441% 5 25.734 2248 2254 2265 rBV2 1013180 2115945 93.36% 19.084%

6 30.810 2802 2807 2812 rBV 129608 237246 10.47% 2.140% 7 33.803 3126 3133 3147 rBV 712016 1533972 67.68% 13.835% 8 38.081 3591 3599 3617 rBV 391188 1156606 51.03% 10.432%

Sum of corrected areas: 11087620

1225.D GCMS0208.M Wed Feb 20 14:30:36 2002

NYC-WTC_000052820

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NYC-WTC_000052820Source: NYC Law Department, mirrored locally

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