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GCMS analysis report for sample AE01042, Feb 2002

Machine-extracted title · confidence 50%

GC/MS analysis report for sample AE01042 showing surrogate recovery data generated on February 27, 2002.

NYC-WTC_000052770–000052776

Folder label: “GCMS X 1/15/02 A 2/11/02

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Scanned page image, NYC-WTC_000052775
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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1102\1042.D Vial: 29 . Acq On : 12 Feb 2002 1:25 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.348 790 796 809 rVB 636414 1616141 76.97% 15.179% 2 15.993 1187 1193 1202 rBV 960689 1974059 94.02% 18.540% 3 21.308 1765 1772 1784 rBV 1040764 2099601 100.00% 19.720% 4 25.751 2250 2256 2267 rBV2 955894 2052053 97.74% 19.273% 5 30.837 2805 2810 2815 rBV 142474 277249 13.20% 2.604%

6 33.830 3129 3136 3150 rBV 669698 1526888 72.72% 14.341% 7 38.117 3595 3603 3624 rBV2 363007 1101314 52.45% 10.344%

Sum of corrected areas: 10647305

1042.D GCMS0208.M Tue Feb 19 10:34:17 2002

NYC-WTC_000052775

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NYC-WTC_000052775Source: NYC Law Department, mirrored locally

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