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GCMS analysis results for sample AE00945, February 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00945 conducted on February 26, 2002.

NYC-WTC_000052693–000052700

Folder label: “GCMS X 1/15/02 A 2/11/02

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Scanned page image, NYC-WTC_000052698
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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1102\945.D Vial: 19 Acq On : 12 Feb 2002 3:43 am Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.343 790 795 810 rVB 873918 2064040 74.34% 14.189% 2 15.987 1186 1192 1209 rBV 1294540 2561367 92.25% 17.607% 3 21.303 1765 1771 1788 rBV 1390783 2776545 100.00% 19.086% 4 25.755 2249 2256 2267 rBV2 1339879 2766782 99.65% 19.019% 5 30.832 2804 2809 2814 rBV 210045 393189 14.16% 2.703%

6 33.825 3128 3135 3154 rBV2 1003295 2245471 80.87% 15.436% 7 38.112 3594 3602 3623 rBV2 581362 1739868 62.66% 11.960%

Sum of corrected areas: 14547262

945 .D GCMS0208.M Tue Feb 19 10:36:38 2002

NYC-WTC_000052698

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NYC-WTC_000052698Source: NYC Law Department, mirrored locally

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