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GCMS calibration table for TCLP analysis, February 2002

Machine-extracted title · confidence 100%

Calibration record for GC/MS instrument 209 used in TCLP testing, listing standard compounds and response factors from February 14, 2002.

NYC-WTC_000052707–000052713

Folder label: “GCMS X 1/15/02 A 2/11/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1102\831.D Vial: 21 Acq On : 12 Feb 2002 5:39 am Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.947 203 207 216 rBV2 12723 32520 1.36% 0.267% 2 12.345 790 795 810 rVB 709594 1800132 75.25% 14.806% 3 15.990 1186 1192 1209 rBV 1134108 2226635 93.08% 18.314% 4 21.305 1765 1771 1782 rBV 1180149 2392113 100.00% 19.676% 5 25.758 2249 2256 2268 rBV 1074854 2328368 97.34% 19.151%

6 30.834 2804 2809 2814 rVB 139078 266342 11.13% 2.191% 7 33.827 3128 3135 3153 rBV 819264 1802696 75.36% 14.828% 8 38.114 3593 3602 3615 rBV2 436629 1308981 54.72% 10.767%

Sum of corrected areas: 12157787

831.D GCMS0208.M Tue Feb 19 10:35:17 2002

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NYC-WTC_000052710

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NYC-WTC_000052710Source: NYC Law Department, mirrored locally

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