GCMS analysis results for sample AE00005, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00005 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050088–000050098

Folder label: “GCMS X 1/3/02 A 1/24/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN2402\5.D Vial: 12 Acq On : 24 Jan 2002 11:51 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time.: Feb 8 11:40 2002 Quant Results File: GCMS0103.RES

Quant Methoci' .: C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title 3": 209 625/TCLP calibration table Last Update " : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.49 152 961717 20.00 ug/1 -0.04 10) Naphthalene-d8 15.08 136 3766200 20.00 ug/1 -0.04 17) Acenaphthene-diO 20.35 164 1900747 20.00 ug/1 -0.04 29) Phenanthrene-diO 24.76 188 2667676 20.00 ug/1 -0.04 38) Chrysene-dl2 32.78 240 1689333 20.00 ug/1 -0.05 44) Perylene-dl2 36.84 264 1179431 20.00 ug/1 -0.05

System Monitoring Compounds 37) 2,4-DDD 29.84 235 138092 4.51 ug/mL -0.23 Spiked Amount 5.000 Recovery = 90.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.14 128 583 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.85 165 280 N.D. 25) Diethylphthalate 21.88 149 231 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 5.D GCMS0103.M Fri Feb 08 11:40:57 2002 Page 1

NYC-WTC_000050090

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000050090Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis results for sample AE00107, Feb 13 2002 · Box DEP Box 28

NYC-WTC_000050145

Laboratory report documenting GCMS analysis of sample AE00107 with detection of unknown compounds and surrogate recovery.

1 shared topics · Same agency, volume and box · similarity 0.998