NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN2402\10.D Vial: 13
Acq On : 25 Jan 2002 12:50 am Operator: 209 GALOS
Sample : GC/MS SCAN 1/3 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 8 11:42 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M.(RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon Jan 07 10:31:02 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.48 152 918393 20.00 ug/1 -0.05
10) Naphthalene-d8 15.08 136 3569558 20.00 ug/1 -0.04
17) Acenaphthene-diO 20.34 164 1796833 20.00 ug/1 -0.05
29) Phenanthrene-diO 24.76 188 2471650 20.00 ug/1 -0.05
38) Chrysene-dl2 32.79 240 1494976 20.00 ug/1 -0.05
44) Perylene-dl2 36.85 264 980345 20.00 ug/1 -0.05
System Monitoring Compounds
37) 2,4-DDD 29.83 235 120894 : 4.26 ug/mL -0.24
Spiked Amount 5.000 Recovery 85.20%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.13 74 108 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.13 128 535 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.79 165 184 N.D.
25) Diethylphthalate 21.87 149 443 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
10 .D GCMS0103 .M Fri Feb 08 11:42:54 2002 Page 1
NYC-WTC_000050137
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