GCMS analysis report for sample AE01036, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\ DATA\ FEB 110 2 \ 10 3 6 . D vial: 24 Acq On : 12 Feb 2002 8:34 am Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Pentenal, (E)- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.93 0.45 ug/1 49219 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentenal, (E)- 84 C5H80 001576-87-0(78 2 2-Pentyn-l-ol 84 C5H80 006261-22-9 50 3 2-Butenal, 3-methyl- 84 C5H80 000107-86-8 45 4 3-Butenenitrile 67 C4H5N 000109-75-1 40 Abundance Scan 206 (6.933 min): 1036.D (-) m/z 83.95 100.00% Si- 39 55 5000

50

m/z-> 20 25 30 —4 +74 ++ Lmmn 35 40 44 ,

45 50 55 60 65 69 -PPPP— 70 75 80 85 6.60 1........... . ' m/z 90 6.80 3 9.05 7.00 7.20 74.72% Abundance #567: 2-Pentenal. (£)- 55

27 5000 39 , Ao6.80, . - , 6.60 7.00 7.20 m/z 41.05 74.03% 51 1 :1, 66 65 ■ ■ • ।'11111 ■ ■ i ■ ■ ■ ■ i ■' TPWTTLTLPLTLTTITITTTTITT । • • • • । • • ■ ■ । m/Z->_ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance 39 55 — 83 6.60 6.80 7.00 7.20 _ 5000 27 m/z 55.00 67.10% 44 51 66 ■ ■' i' ■ ■ ■ i' ■' ■ i'''' i'' ' ■ i'' ■' 48 i ■ ■■' r ' • ■ i '' ■ ' i ■'' ■ i ‘ ■ ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i ■ ■1 ■ i ■ •'' i ■

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62726: 2-Butenal, 3-methyl- ---AITT 84 6.60 6.80 7.00 7.20_____ m/ Z 83.0.5 49.21% 5000 41 55

50 , m/z-> ■ । ■' ■ ■ ।'1111 ■''1111111 20 25 30 35 40 TdT 45 ' 11 ' ।' 50 55 T60P65§65170.......... hp 75 80 85 90 6.60 6.80 7.00 7.20

1036.D GCMS0208.M Tue Feb 19 10:31:25 2002 Page 2

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