GCMS analysis report for sample AE01036, Feb 2002

NYC 9/11 Public Portal Document

Data File : C : \HPCHEM\ 1 \DATA\FEB1102\1036.D Vial: 24 Acq On : 12 Feb 2002 8:34 am Operator: 209 GALOS Sample : GC/MS SCAN 1/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopropanecarboxylic acid Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.24 0.37 ug/1 40399 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 MW MolForm CAS# Qual

1 Cyclopropanecarboxylic acid 86 C4H602 001759-53-1 2 Methacrylamide 85 C4H7NO 000079-39-0 42 3 Furan, 2,5-dihydro- 70 C4H60 001708-29-8 12 4 Allyl chloroformate 120 C4H5C1O2 002937-50-0 12 Abundance Scan ‘3 (6 244 min): 1036. D (-) m/z 84.95 100.00% eh

5000 60 f..........

m/z-7 5 ■ ■ i ■ 10 1’7 I I | I ! I I | I I I ! | 15 20 25 30 a. t;7.. .1. ,

35 40 45 50 55 60 65 70 57 V" FT’It .........."'I 75 80 85 90 m/z 6.00 6.20 41.05 6.40। 6.60 99.40% Abundance #655: Cyclopropanecarboxylic acid 3k

5000 42 58 85 ■ (■ ■ had Proego6.20 _____ 6.00 6.40 6.60 27 45 68' m/z 42.95 70.08% 71 '1' ■ i ■ 111 ' I " " 11 " 11 i1" ' r " ' i " " i " " i" " i m/Z-? 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance 85 41

44 _ 6.00 6.20 6.40 6.60 5000 63 m/z 39.05 52.68% 38 53 66 r 'r r b ■ ■ r " ■ r'' ■ i • ■ " i ■ " ' i TTUTTTT i " ■ ■ i " '' r ■' ■ r ''' i ■ i ■ ■ i ■ mfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62432: Furan, 2.5-dihydro- 39 —AAAAAAALAA 6.00 6.20 6.40 6.60 12 m/z 41.95...... 3 2.62 % 70 5000

27 15 1 30 34 H A M ] I ' ' ' ' I i " " i " " i ++ ■ I ’' " 11 i" ’ ■ i miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.00 6.20 6.40 6.60

1036.D GCMS0208.M Tue Feb 19 10:31:20 2002 Page 1

NYC-WTC_000052733