GCMS analysis log for sample AE00704 showing surrogate recovery and unknown compounds detected on January 29, 2002.
NYC-WTC_000051914–000051929Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
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Data File : C:\MSDCHEM\1\5973N\02JAN16\00704.D Vial: 4 Acq On : 16 Jan 2002 5:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 dl-Limonene $$ Cyclohexene,... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 10.10 0.26 ug/L 90650 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# . Qual
1 dl-Limonene $$ Cyclohexene, 1-me... 136 C10H16 000138-86-3 96 2 Cyclohexene, l-methyl-4-(1-methy... 136 C10H16 005989-54-8 95 3 dl-Limonene $$ Cyclohexene, 1-me... 136 C10H16 000138-86-3 95 4 D-Limonene $$ Cyclohexene, 1-met... 136 C10H16 005989-27-5 93 Abundance Scan 589 (10.098 min): 00704.D (-) m/ z 68.10 100.00% 68 93 5000 41 53 79 107 121 136 ’ ddI/aI*’’t 9.80 10.00 10.20 10.40
/z-> 0> । ' > > ' । < 20 30 40 44 50 60 70 80 90 100 110 120 130 140 m/z 93.10 80.44% Abundance #31986: dl-Limonene $$ Cyclohexene, 1-methyl-4-(1-methylet... 63 93
5000 79 9.80 L ' 11 1 10.00 10.20 10.40 T 53 107 121 136 m/z 75.82% 67.10 o1. । ■ .. . । . ' ■ . । . . . . । । । । . ----- •11 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #32009: Cyclohexene, 1-methyl-4-(1 -methylethenyl)-, (S)- 68 9.80 10.00 10.20 10.40 93 m/ z 79.10 29.09% 5000 53 79 27 ..................... 107 121 136 0 ' I ' ' ' ' I ' ' 1 ' I ' ' 1 1 1 1 ' 1 1 1 1 1 1 I I 1 1 i ‘ ■ ■ ■ i 1 1 ■ ' i ' ■ ' r i ‘ ■ l ■ i ■ ■
m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #31999: dl-Limonene $$ Cyclohexene, 1-methyl-4-(1-methylet... . ....... A.......... 68 9.80 10.00 10.20 10.40 m/ z 94.10 28.79% 93 5000 79 27 53 136 107 121
0 I 111111 • ■ । ' I 1 1 ‘ 1 i * I > I । । । । I । । 1 ' I /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 9.80 10.00 10.20 10.40
)0704.D SCAN508.M Thu Jan 17 08:17:35 2002 Page 9
NYC-WTC_000051926
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NYC-WTC_000051531
Laboratory report showing GCMS analysis results for sample AE00555 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050683
Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051624
Laboratory report showing GCMS analysis results for sample AE00615 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051895
GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006206
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03251 conducted on March 15, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
Filed in the same folder