GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
NYC-WTC_000051877–000051894Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02JAN16\00701 .D Vial: 1 , Acq On : 16 Jan 2002 3:07 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************** Peak Number 9 D-Limonene Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 10.10 1.67 ug/L 516996 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 D-Limonene 136 C10H16 005989-27-5 98 2 Cyclohexene, l-methyl-4-(1-methy... 136 C10H16 005989-27-5 97 3 Limonene $$ Cyclohexene, 1-methy... 136 C10H16 000138-86-3 97 4 di-Limonene $$ Cyclohexene, 1-me... 136 C10H16 000138-86-3 97 Abundance Scan 589 (10.098 min): 00701 D (-) m/ z 68.10 100.00% 68 93
5000
41 53 79 107 121 136 J i ‘ ■ ■ i TCr‘ 1 ' 1
■n/z-> 0 30 l+ 40 501 60 .......................... . 70 80 90 100 1,1,115...... 11 I 1 I 1 1 I ' ' ' I I ' I ' I I I I 110 120 130 140 m/z 9.80 10.00 10.20 10.40 67.10 69.35% Abundance #31979: D-Limonene 63
5000 93 TB7 T"T y 9.80 10.00 10.20 10.40 53 79 107 121 136 m/z 93.10 67.82%
0T • i ■ • ■ ■ i ■ • • • i ■ rv I|i..... I,... ' I ' 1 1 1 1 1 1 11 I ' ' n/z-> 30 40 50 60 70 90 100 110 120 130 140 Abundance #31985: Cyclohexene, 1-methyl-4-(1-methylethenyl)-, (R)- (... 6)3 —I l . f 9.80 10.00 10.20 10.40 93 m/z 79.10 31.12% 5000
53 79 136 107 121 - /z-> 0i ■ ■ ■ ' i ' 1 1 ■ i ■ ■ 1 1 I 1 1 30 40 50 60 70 .... ll80.....90I 100 110 120 130 140 Abundance #31988: Limonene $$ Cyclohexene, 1-methyl-4-(1-methylethen... < 1 > | 1 > 1 » | 1'■ e • | C ■ r 1 | i -i -r r | 68 9.80 10.00 10.20 10.40 m/z 94.10 29.06% 93 5000
53 79 107 121 136 0 I ' 1 1 1 1 1 ' 1 1 1 1 1 1 1 1 1 I - i ■ ■ ■ • i Ti n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 9.80 10.00 1020 10.40
30701.D SCAN508.M Thu Jan 17 08:17:17 2002 Page 11
NYC-WTC_000051891
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NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051895
GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051860
GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051948
Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051697
Laboratory report showing GCMS analysis results for sample AE00470 conducted on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
Filed in the same folder