Laboratory report documenting a method blank analysis to verify absence of contamination during gas chromatography-mass spectrometry testing.
NYC-WTC_000051353–000051363Folder label: “GCMS X 1/8/02 A 1/11/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN14\0108BA.D Vial: 1 Acq On : 14 Jan 2002 10:28 am Operator: Sample : lab blank 1/8 a Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L **************************************************************** * * *** Peak Number 4 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 61196 Phenanthrene-dlO 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H12O3 004497-40-9 45 Abundance Scan 1656 (22.280 min): 0108BA.D (-) m/z 192.10 100.00% 192
5000
82 96 146 160 22.00 22.20 22.40 22.60
/z-> 0 . ......... . 70 i". ■ !■ .1 +P Pp 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.10 19.23% Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
108 5000 22.00 22.20 22.40 22.60 146 175 m/z96.00 14.39%
0 i " " i " " i " " i" ' i " " i" " i' Iapastui I, r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 0 11 1 1 — 22.00 22.20 22.40 22.60 5000 82 m/z 146.10 13.67%
54 110 30 I 94 160 Ojumn......... 1 ■ i' " 1 r 11 • 111" । I' । . —TTTTp Tp-1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102610: 2-Propenal, 3-(3,4-dimethoxyphenyl)- (CAS) $$ 3.4... 192 C 22.00 22.20 22.40 22.60 161 m/z 82.00 12.19%
5000
77 149 177 64 89 193 118 138 0 {■ ■ ■11 ■ > > 11 • > > > I ■ I I r ''' i1''' i'' i • " ' i I’T " I ‘1111 1m - m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
3108BA.D SCAN508.M Tue Jan 15 08:47:58 2002 Page 6
NYC-WTC_000051361
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NYC-WTC_000049891
Laboratory report showing blank analysis results with concentrations below method detection limits for various organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051055
Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051088
Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051040
Laboratory report showing GCMS analysis of sample AE00276 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049929
Laboratory report showing GCMS analysis of sample AD31637 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051073
Laboratory report showing GCMS analysis of sample AE00308 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051422
Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051010
Blank analysis report for GCMS of sample AE00275 showing compounds below method detection limits from January 8-10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051471
Laboratory report showing GCMS analysis of sample AE00469 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051137
Laboratory report showing GCMS analysis of sample AE00320 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051439
Laboratory report showing GCMS analysis of sample AE00464 with surrogate recovery data on January 24, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049916
Laboratory report showing GCMS analysis of sample AD31631 including unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051336
Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.
Filed in the same folder
NYC-WTC_000051337
Administrative label page identifying the folder range for gas chromatography-mass spectrometry records from January 8 to January 11, 2002.
Filed in the same folder
NYC-WTC_000051338
Instrument output showing total ion chromatogram and abundance data for dodecafluorotriphenylphosphine (DFTPP) calibration on January 11, 2002.
Filed in the same folder
NYC-WTC_000051340
Laboratory report listing concentrations of volatile organic compounds including nitrosamines and chlorinated solvents in sample AE00314.
Filed in the same folder
NYC-WTC_000051344
Second calibration standard report for gas chromatography-mass spectrometry analysis of sample AE00314 conducted on January 15, 2002.
Filed in the same folder