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GCMS blank analysis for sample AE00314, Jan 15 2002

Machine-extracted title · confidence 100%

Laboratory report documenting a method blank analysis to verify absence of contamination during gas chromatography-mass spectrometry testing.

NYC-WTC_000051353–000051363

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051362
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN14\0108BA.D Vial: 1 Acq On : 14 Jan 2002 10:28 am Operator: Sample : lab blank 1/8 a Inst : Instrumen Mise January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ***************************************************************** * ** * Peak Number 5 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.27 ug/L 128906 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-dlO 188 C14D10 001517-22-2 87 3 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 83 4 C14 H2 0 hydrocarbon 188 C14H20 000000-00-0 53 Abundance Scan 1699 (22.771 min): 0108BA.D (-) m/z 188.15 100.00% 188

5000

80 94 ......it- T' ' 1 ■ I ' ' ' ' I ' 22.40 22.60 22.80 23.00 23.20

mlz-> 40 0 ""I"' 30 40 50 - 66 11 rri T i' TIT 156 11" " i"111"' H " " i'1 60 70 80 90 100 110 120 130 140 150 160 170 180 190 —l m/z 94.10 18.21% Abundance #84502: Anthracene-d10- 188

5000 22.40 22.60 22.80 23.00 23.20 m/z 184.10 17.54% 80 94 160 66 OfTTTTTT L r " ' i' • " i " " i ■ ■ 1801, n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 r^rr

Abundance #84499: Phenanthrene-d10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 189.10 14.45%

80 94 160 66 - - Op TTTTTTT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 ......................... ............................ 188 22.40 22.60 22.80 23.00 23.20 m/z 80.00 13.36%

5000

80 94 66 158 — Orr UIWtgr ... i"1H " " ।'1 '111'' ■ i'' ■' i' ■'' i''' i ----------------------- m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1 70 180 190 22.40 22.60 22.80 23.00 23.20

0108BA.D SCAN508.M Tue Jan 1-5 08:47:58 2002 Page 7

NYC-WTC_000051362

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NYC-WTC_000051362Source: NYC Law Department, mirrored locally

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