GCMS analysis results for sample AE00318, Jan 2002

NYC 9/11 Public Portal Document

Llprary Search compound Keporc

Data File C: \MSDCHEM\1\5973N\02JAN08\318.D Vial: 3 Acq On 8 Jan 2002 7:06 pm Operator: Sample 508scan Inst : Instrumen Mise January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.49

Hit# of 0.20 ug/L

5 Tentative ID 69533 1,4-Dichlorobenzene-d4

MW MolForm CAS# 9.72 Y M AV Qual". 1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 59 Abundance Scan 10 (3.488 min): 318. D (-) m/z 74.00 100.00% 74 82 5000 47 TTrrrpr, 86

/z—> 0 35 ■ ■ i < < 111 > । H i ■ > ■ 11 ■ I""r"'i T 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 TTT Xu ।''' ■ । ■r ■ । TTT 3.50 3.60 3.70 3.80 3.90 m/ z 81.90 61.17% Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 47 82 5000 3.50 3.60 3.70 3.80 3.90 38 m/z 76.00 33.96% 95 102 108 0 "i""r ' i " ’ ■ i' 'I... .> .... ... i"111" " i" " i ‘ it — /z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 83.95 30.00% 47 35

/z—> 0 ....al..... .... ri" " i" " i" " i11' "TTT 109 ' i" " i" " r1" i"111" " i 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #11644: Acetonitrile, dichloro- 74 3.50 3.60 3.70 3.80 3.90 35 m/z 47.00 26.67% 5000 82 47 10 0 " I" mip +— np- TT+ i " " |" i " " r " ■ i " 1' i " 11 1 1 1 1 1 I"'1 ’ | ■ 1 1 1 1 m/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 3.50 3.60 3.70 3.80 3.90

318.D SCAN508.M Wed Jan 09 15:17:41 2002 Page 3

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