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GCMS analysis results for sample AE00307, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051055–000051072

Folder label: “GCMS X 1/7/02 A 1/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN08\307.D Vial: 6 Acq On : 8 Jan 2002 9:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 8 2-Propanol, 1-(2-methoxypro. . . Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

9.85 0.13 ug/L 42091 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 74 2 Butanoic acid, 2-hydroxy- $$ But... 104 C4H803 000565-70-8 9 3 Methane, diethoxy- $$ Ethane, 1,. 104 C5H12O2 000462-95-3 7 4 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 4 Abundance Scan 567 (9.847 min): 307.D (-) m/z 59.10 100.00% 59

5000

0 73 86 —I i | | Ji i ! | | | I . । 104 ।.I । । ।. —, N y . . . m/ z 9.60 9.80 45.00 10.00 10.20 14.68% mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 A Abundance #43942: 2-Propanol, 1 -(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 9.60 9.80 10.00 10.20 m/z 43.00 11.91% 31 45 73 <04 01 • i ■ ■ ------ . , 7 , 130 /z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #10063: Butanoic acid, 2-hydroxy- $$ Butyric acid, 2-hydro... 31 59 1 'T' ' 9.60 10.00 10.20 9.80 5000 m/z 41.10 10.95%

45 76

n/z-> Abundance 0 ■ i ' ■ 20 rT 30 31 H 1*... . ..... . ■ i ■ 40 50 60 70 80 90 100 104

110 120 #10228: Methane, diethoxy- $$ Ethane, 1,1'-[methylenebis(o... 50 130 _MM_ m/z 9.60 9.80 73.00 10.00 10.20 9.75% 103 5000

47 OPp 1 । 1 i ' 1 ' 1 1 ' 1L It..... 1— i 75 89 11 N, A.A..... m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

307.D SCAN508.M Wed Jan 09 15:16:57 2002 Page 10

NYC-WTC_000051068

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NYC-WTC_000051068Source: NYC Law Department, mirrored locally

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