GCMS analysis results for sample AE00275, Jan 2002

NYC 9/11 Public Portal Document

yuantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN08\0108C40.D Vial: 3 * Acq On 8 Jan 2002 10:20 am Operator: Sample : cal 40 Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 09 12:51:20 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Wed Jan 09 12:49:14 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1144488 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 5148602 20.00 ug/L -0.01 17) Acenaphthene-dlO 18.34 164 2650543 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.66 188 4525529 20.00 ug/L -0.01 38) Chrysene-dl2 30.51 240 3893525 20.00 ug/L 0.00 44) Perylene-dl2 34.43 264 2937756 20.00 ug/L 0.01

System Monitoring Compounds 37) 2,4-DDD 27.57 235 34697 0.49 ug/L—>-0.16 Spiked Amount 5.000 Recovery 1 9.80% -< x Target Compounds Qvalue 2) w-nitroso-dimethylamine 3.98 74 2034951 41.72 ug/L 54 3) bis A(2-Chloroethyl )A ether 9.26 93 2729615 37.54 ug/L 78 4) 1,3-Dichlorobenzene 9.62 146 3154109 36.73 ug/L 96 5) 1,4-Dichlorobenzene 9.77 146 3126856 36.26 ug/L 98 6) 1,2-Dichlorobenzene 10.25 146 2653401 34.65 ug/L 99 7) 2,2 ' -oxybis s(1-Chloropropa 10.68 45 4480693 33.85 ug/L 95 8) N-nitroso-di-n-propylamine 11.08 70 1950555 32.29 ug/L 85 9) Hexachloroethane 11.03 117 1084852 35.14 ug/L 98 11) Nitrobenzene 11.38 77 3144194 32.70 ug/L 85 12) Isophorone 12.04 82 5999110 34.59 ug/L 94 13) bisX(2 -Chloroethoxy) metha 12.79 93 3907889 37.91 ug/L 93 14) 1,2,4-Trichlorobenzene 13.12 180 2383749 35.51 ug/L 98 15) Naphthalene 13.26 128 8825057 35.78 ug/L 99 16) Hexachlorobutadiene 13.85 225 1151612 32.26 ug/L 98 18) Hexachlorocyclopentadiene 15.96 237 953304 40.24 ug/L 98 19) 2-Chloronaphthalene 16.67 162 5112725 34.93 ug/L 93 20) Dimethylphthalate 17.92 163 5754705 32.88 ug/L 94 21) 2,6-Dinitrotoluene 18.09 165 1411757 41.35 ug/L 76 22) Acenaphthylene 17.88 152 7847009 36.76 ug/L 97 23) 24) Acenaphthene 2,4-Dinitrotoluene 18.44 19.21 153 165 4754297 1966286 <31.27 ug/L 43.98 ug/L 100 93 25) Diethylphthalate 20.03 149 5320879 31.72 ug/L 99 26) 4-Chlorophenyl-phenylether 20.04 204 2300454 32.63 ug/L 91 27) Fluorene . 19.93 166 6004746 34.72 ug/L 98 28) Azobenzene/l,l-biruot‘Myazas 20.49 77 7084829 33.88 ug/L 89 30) N-nitrosodiphenylamine 20.46 169 3860561 33.63 ug/L 98 31) 4-Bromophenyl-phenylether 21.46 248 1592926 33.82 ug/L 88 32) Hexachlorobenzene 21.79 284 1678529 33.73 ug/L 99 33) Phenanthrene 22.73 178 8634895 34.62 ug/L 100 34) Anthracene 22.85 178 8736290 36.11 ug/L 99

(#) = qualifier out of range (m) = manual integration 0108C40.D SCAN508.M Wed Jan 09 12:51:21 2002 1 Page 1

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