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GCMS analysis results for sample AE00166, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.

NYC-WTC_000050683–000050701

Folder label: “GCMS X 1/4/02 A 2/4/02

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NYC 9/11 Public Portal Document — I.------------------- —ME—*

Data File : C: \MSDCHEM\1\5973N\02FEB04\00166.D Vial: 5 • Acq On 4 Feb 2002 6:27 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area ' Relative to ISTD R.T. 5.90 2.18 ug/L 1367070 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 221 (5.897 min): 00166. D (-) m/z 73.10 100.00% 73

5000 43 1 1 1 ' '‘'I'1 ' • • i ‘ ‘ ‘ 1 5 4 5.60 5.80 6.00 6.20 n/z-> 0- 4l 55 , 87 103 Tt"I ■ i ITfMi 11 ■ ri'i । m 111 >'i i. 11111111 > < 11. ।. 11111 ■ 1111 m > 11 > np 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 43.10 23.60% Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 TTmemuEmOuTTT 5.60 5.80 6.00 6.20 43 m/z 45.10 9.56% 27 0- mm 55..... ,1 , 1’1111137111 87 113 'I i. । . I'. ।, h . ।. 11‘! n 111 > > 11 ■ PTTT 174 ।। ■ i।. miz-> 10 20 30 40 50 O) 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 1 r | i-r-.-i । i 441*** i l » 1 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.85% 43 27 55.... ..I , 87 । r i >->■). i > > 113 174 0- mp ■ । • ■ ■ ■ i ■ ■ ■ ■ i ■ ‘H 1111 । i'i 111111. ।. i m ।. i > > । n . 1111 .. 1111111 niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 1 14T’i ' 1 1‘ ■i ■ 1 73 5.60 5.80 6.00 6.20 m/z 71.10 6.24%

5000

45 1 53 m/z-> 15 0 TIPTTT THnpmp ..1..•88।।...r|..i.।।iij।।।. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Apoe 5.60 5.80 6.00 -r-n-n- 6.20

0166.D SCAN508.M Tue Feb 05 09:47:39 2002 Page 7

NYC-WTC_000050693

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NYC-WTC_000050693Source: NYC Law Department, mirrored locally

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