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GCMS analysis results for sample AE00250, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.

NYC-WTC_000050596–000050614

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050600
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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN24\00250.D Vial: 6 . Acq On : 24 Jan 2002 7:06 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.613 17 21 25 rBV 39549 58909 0.39% 0.069% 2 4.253 73 77 83 rBV4 29061 71592 0.48% 0.084% 3 4.630 103 110 115 rBV 30385 74420 0.50% 0.087% 4 4.835 123 128 141 rBV2 45655 116554 0.78% 0.137% 5 5.018 141 144 149 rW 77632 148217 0.99% 0.174%

6 5.714 201 205 209 rW 72899 121071 0.81% 0.142% 7 5.885 217 220 241 rBV 1046185 2082891 13.86% 2.440% 8 9.721 551 556 561 rW 4842533 9722763 64.69% 11.391% 9 9.858 561 568 577 rW 16242 69119 0.46% 0.081% 10 13.192 855 860 865 rBV 6850670 13759216 91.54% 16.120%

11 18.341 1305 1311 1315 rBV 7122295 14437527 96.05% 16.915% 12 22.280 1653 1656 1661 rVB 56224 111177 0.74% 0.130% 13 22.645 1681 1688 1693 rBV2 6618139 15030523 100.00% 17.609% 14 22.771 1697 1699 1713 rVB 89182 226315 1.51% 0.265% 15 23.810 1785 1790 1797 rW 23231 52992 0.35% 0.062%

16 24.849 1877 1881 1889 rW 22777 49783 0.33% 0.058% 17 27.726 2129 2133 2139 rW 911759 1657791 11.03% 1.942% 18 30.500 2369 2376 2381 rBV 5997794 14469876 96.27% 16.952% 19 31.105 2425 2429 2457 rVB 102625 487417 3.24% 0.571% 20 34.416 2713 2719 2747 rBV 4600763 12607283 83.88% 14.770%

Sum of corrected areas: 85355436

30250.D SCAN508.M Fri Jan 25 10:26:22 2002 Page 1

NYC-WTC_000050600

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NYC-WTC_000050600Source: NYC Law Department, mirrored locally

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