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GCMS results for sample AE00701, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051877–000051894

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00701.D Vial: 1 . Acq On : 16 Jan 2002 3:07 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks : 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 4.846 119 129 139 rBV6 15552 61092 0.56% 0.100% 2 5.006 139 143 149 rVB 26257 47352 0.43% 0.077% 3 5.885 215 220 227 rBV 634380 1244781 11.35% 2.037% 4 7.438 353 356 367 rBV 63807 174390 1.59% 0.285% 5 8.237 423 426 433 rVB 23150 54177 0.49% 0.089%

6 9.527 535 539 545 rBV 55575 133163 1.21% 0.218% 7 9.619 545 547 551 rW 59428 122446 1.12% 0.200% 8 9.710 551 555 561 rW 3230375 6179918 56.37% 10.113% 9 9.824 561 565 583 rVB 70769 215217 1.96% 0.352% 10 10.098 583 589 593 rBV 272002 516996 4.72% 0.846%

11 13.192 855 860 865 rBV 4793700 8843758 80.67% 14.472% 12 18.341 1305 1311 1315 rBV 4851962. 9830359 89.67% 16.087% 13 22.280 1653 1656 1661 rVB2 40984 77034 0.70% 0.126% 14 22.634 1681 1687 1693 rBV2 4936151 10871735 99.17% 17.791% 15 22.771 1693 1699 1703 rVB 53285 135502 1.24% 0.222%

16 24.849 1877 1881 1887 rVB 35458 64603 0.59% 0.106% 17 27.726 2127 2133 2139 rVB 956172 1752429 15.99% 2.868% 18 30.489 2369 2375 2381 rBV2 4522259 10962790 100.00% 17.940% 19 31.105 2425 2429 2441 rW 80393 255732 2.33% 0.418% 20 34.416 2713 2719 2751 rBV 3623282 9565833 87.26% 15.654%

Sum of corrected areas: 61109307

10701.D SCAN508.M Thu Jan 17 08:17:14 2002 Page 1

NYC-WTC_000051881

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NYC-WTC_000051881Source: NYC Law Department, mirrored locally

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