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GCMS results for sample AE00739, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051967–000051983

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00739.D Vial: 7 - Acq On : 16 Jan 2002 8:07 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rVB2 27846 45388 0.36% 0.063% 2 4.241 71 76 83 rW5 22808 57922 0.46% 0.080% 3 4.618 107 109 119 rVB2 20201 42724 0.34% 0.059% 4 4.778 119 123 125 rBV 23205 34771 0.28% 0.048% 5 4.823 125 127 129 rBV2 31055 50048 0.40% 0.069%

6 5.006 139 143 147 rVB2 31924 66918 0.53% 0.092% 7 5.885 217 220 243 rVB 786235 1707025 13.53% 2.356% 8 7.426 351 355 367 rBV 168975 440565 3.49% 0.608% 9 8.225 423 425 435 rBV 85494 198407 1.57% 0.274% 10 9.710 551 555 561 rBV 3790843 7353050 58.27% 10.150%

11 13.192 855 860 865 rBV 5590370 10700619 84.80% 14.771% 12 18.341 1305 1311 1315 rBV 5963307 11810093 93.59% 16.303% 13 21.332 1569 1573 1577 rW 22399 40506 0.32% 0.056% 14 22.280 1653 1656 1661 rVB2 53828 95686 0.76% 0.132% 15 22.645 1681 1688 1693 rW2 5588865 12618743 100.00% 17.419%

16 22.771 1693 1699 1715 rW 72195 236093 1.87% 0.326% 17 27.726 2129 2133 2139 rBV 1018346 1855871 14.71% 2.562% 18 30.488 2369 2375 2381 rBV 4627972 11707624 92.78% 16.161% 19 33.411 2625 2631 2679 rBV 694660 3449454 27.34% 4.762% 20 34.416 2713 2719 2737 rBV 3825997 9930026 78.69% 13.708%

Sum of corrected areas: 72441533

)0739.D SCAN508.M Thu Jan 17 08:17:51 2002 Page 1

NYC-WTC_000051971

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NYC-WTC_000051971Source: NYC Law Department, mirrored locally

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