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GCMS analysis results, sample AE00738, January 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.

NYC-WTC_000051948–000051966

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00738.D Vial: 6 . Acq On : 16 Jan 2002 7:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.006 139 143 147 rBV 52235 94703 0.80% 0.144% 2 5.885 217 220 249 rVB 707713 1515441 12.79% 2.309% 3 7.438 351 356 367 rBV 76063 216050 1.82% 0.329% 4 8.226 421 425 435 rVB 38666 97433 0.82% 0.148% 5 9.539 537 540 545 rBV 37481 79848 0.67% 0.122%

6 9.630 545 548 551 rW 38253 79272 0.67% 0.121% 7 9.710 551 555 561 rW 3636893 6988552 58.97% 10.649% 8 9.836 561 566 575 rVB 40373 107220 0.90% 0.163% 9 13.192 855 860 865 rBV 5349079 10097764 85.20% 15.386% 10 18.341 1305 1311 1315 rBV 5575628 11017026 92.96% 16.787%

11 22.280 1653 1656 1663 rVB2 47718 90421 0.76% 0.138% 12 22.634 1681 1687 1693 rBV2 5324665 11851221 100.00% 18.058% 13 22.771 1693 1699 1707 rVB 63916 187026 1.58% 0.285% 14 27.726 2129 2133 2137 rBV 950075 1702505 14.37% 2.594% 15 30.489 2369 2375 2381 rBV2 4664096 11379384 96.02% 17.339%

16 31.105 2425 2429 2445 rVB 56499 207798 1.75% 0.317% 17 33.263 2613 2618 2625 rW5 19584 67283 0.57% 0.103% 18 34.119 2689 2693 2703 rBV2 29377 115310 0.97% 0.176% 19 34.416 2713 2719 2753 rVB 3744725 9638291 81.33% 14.686% 20 34.930 2761 2764 2777 rBV 25388 96347 0.81% 0.147%

Sum of corrected areas: 65628895

30738.D SCAN508.M Thu Jan 17 08:17:45 2002 Page 1

NYC-WTC_000051952

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