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GCMS results for sample AE00702, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051895–000051913

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00702.D Vial: 2 . Acq On : 16 Jan 2002 3:57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 4.824 125 127 137 rBV 37950 99004 0.77% 0.130% 2 5.885 215 220 227 rBV 829714 1637735 12.75% 2.158% 3 6.000 227 230 235 rVB 52919 111019 0.86% 0.146% 4 7.427 353 355 375 rW 104904 263856 2.05% 0.348% 5 9.527 535 539 545 rBV2 48928 119298 0.93% 0.157%

6 9.619 545 547 551 rW 44823 96094 0.75% 0.127% 7 9.710 551 555 561 rW 3909109 7337350 57.13% 9.668% 8 9.824 561 565 575 rVB 58831 146304 1.14% 0.193% 9 10.098 585 589 593 rVB 237660 450461 3.51% 0.594% 10 13.192 855 860 865 rBV 5609183 10511236 81.84% 13.850%

11 18.341 1305 1311 1315 rBV 5914567 11771200 91.65% 15.510% 12 22.280 1651 1656 1661 rBV 53465 102670 0.80% 0.135% 13 22.645 1681 1688 1693 rBV2 5548861 12842992 100.00% 16.923% 14 22.771 1693 1699 1703 rVB 66988 164519 1.28% 0.217% 15 27.726 2129 2133 2139 rBV 1142207 2059235 16.03% 2.713%

16 30.500 2369 2376 2381 rBV 4875603 12379306 96.39% 16.312% 17 31.105 2425 2429 2451 rVB 127011 412893 3.21% 0.544% 18 33.412 2625 2631 2671 rW 1028120 4468421 34.79% 5.888% 19 34.119 2687 2693 2703 rBV3 32497 116079 0.90% 0.153% 20 34.416 2713 2719 2747 rVB 4120897 10802559 84.11% 14.234%

Sum of corrected areas: 75892231

)0702.D SCAN508.M Thu Jan 17 08:17:21 2002 Page 1

NYC-WTC_000051899

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NYC-WTC_000051899Source: NYC Law Department, mirrored locally

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