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GCMS results for sample AE00737, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051930–000051947

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051934
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00737.D Vial: 5 . Acq On 16 Jan 2002 6:26 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 23 rBV 32618 42778 0.33% 0.060% 2 4.241 71 76 83 rW3 36777 81900 0.64% 0.114% 3 4.618 107 109 123 rVB2 25746 56098 0.44% 0.078% 4 4.823 123 127 141 rVB2 44928 119766 0.93% 0.167% 5 5.006 141 143 149 rBV2 23064 42025 0.33% 0.058%

6 5.885 217 220 245 rBV 854886 1776612 13.86% 2.473% 7 7.438 353 356 367 rBV 70834 190418 1.49% 0.265% 8 8.226 423 425 437 rW 39484 99196 0.77% 0.138% 9 9.710 551 555 561 rW 3963096 7560541 58.98% 10.524% 10 9.847 561 567 577 rW 16747 61964 0.48% 0.086%

11 10.098 585 589 595 rW3 26525 50239 0.39% 0.070% 12 13.192 855 860 865 rBV 5647162 10836162 84.53% 15.084% 13 18.341 1305 1311 1315 rBV 6002574 11956179 93.26% 16.643% 14 22.280 1651 1656 1661 rW 54101 95207 0.74% 0.133% 15 22.645 1681 1688 1693 rBV 5622881 12819871 100.00% 17.845%

16 22.771 1695 1699 1713 rW 74835 219095 1.71% 0.305% 17 27.726 2129 2133 2139 rW 1133922 2087463 16.28% 2.906% 18 30.489 2369 2375 2381 rBV 4980842 12700127 99.07% 17.678% 19 31.105 2419 2429 2435 rBV8 12629 60434 0.47% 0.084% 20 34.416 2713 2719 2745 rBV 4302631 10984729 85.69% 15.290%

Sum of corrected areas: 71840804

)0737.D SCAN508.M Thu Jan 17 08:17:38 2002 Page 1

NYC-WTC_000051934

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NYC-WTC_000051934Source: NYC Law Department, mirrored locally

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