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GCMS analysis results for sample AE00167, Jan 2002

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Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050481–000050499

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN24\00167.D Vial: 4 . Acq bn : 24 Jan 2002 2:09 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.488 5 10 15 rBV 85624 136162 0.86% 0.157% 2 3.613 19 21 25 rVB 39572 59517 0.38% 0.069% 3 4.253 73 77 83 rVB4 18965 51991 0.33% 0.060% 4 4.629 103 110 119 rBV2 22919 58819 0.37% 0.068% 5 4.846 123 129 137 rBV2 25110 74271 0.47% 0.086% 6 5.018 141 144 149 rBV 39611 66972 0.42% 0.077% 7 5.885 217 220 227 rBV 1076048 1975320 12.46% 2.276% 8 5.999 227 230 235 rVB 123850 255532 1.61% 0.294% 9 9.721 551 556 561 rW 4939161 9739244 61.42% 11.224% 10 9.858 561 568 577 rVB2 11617 39936 0.25% 0.046% 11 13.192 855 860 865 rBV 6801106 13819766 87.16% 15.927% 12 18.341 1305 1311 1317 rBV 7209305. 14921876 94.11% 17.197% 13 22.280 1653 1656 1661 rW2 63909 127342 0.80% 0.147% 14 22.645 1681 1688 1693 rBV2 7053171 15855855 100.00% 18.273% 15 22.771 1695 1699 1711 rVB 93972 262030 1.65% 0.302% 16 26.013 1977 1983 1987 rBV 30690 67943 0.43% 0.078% 17 27.726 2127 2133 2139 rBV 1045645 1864324 11.76% 2.149% 18 30.500 2369 2376 2381 rBV 6037932 14674202 92.55% 16.911% 19 31.105 2425 2429 2441 rVB4 11250 47555 0.30% 0.055% 20 34.416 2713 2719 2757 rBV 4520186 12671913 79.92% 14.604%

Sum of corrected areas: 86770570

0167.D SCAN508.M Fri Jan 25 10:25:46 2002 Page 1

NYC-WTC_000050485

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