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GCMS results for sample AE00557, Jan 17 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00557 showing surrogate recovery and unknown compounds detected on January 17, 2002.

NYC-WTC_000051768–000051781

Folder label: “GCMS X 1/9/02 A 1/15/02

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Scanned page image, NYC-WTC_000051772
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00557.D Vial: 1 Acq On : 15 Jan 2002 1:32 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 5.885 217 220 227 rW 453602 1017307 8.79% 1.661% 2 6.000 227 230 241 rVB 60302 155424 1.34% 0.254% 3 9.048 493 497 505 rVB 24959 53131 0.46% 0.087% 4 9.710 551 555 561 rW 3173148 6385980 55.17% 10.425% 5 9.847 561 567 577 rVB 16680 56906 0.49% 0.093%

6 13.192 855 860 865 rBV 4890029 9223832 79.69% 15.058% 7 18.341 1305 1311 1315 rBV 5285474 10335235 89.29% 16.872% 8 18.433 1315 1319 1329 rVB3 16467 59356 0.51% 0.097% 9 19.997 1451 1456 1469 rVB 37693 87071 0.75% 0.142% 10 20.431 1491 1494 1501 rVB2 26902 73470 0.63% 0.120%

11 22.280 1651 1656 1661 rBV 46072 83471 0.72% 0.136% 12 22.645 1681 1688 1693 rBV 5168993 11574597 100.00% 18.896% 13 22.771 1695 1699 1701 rVB 48601 78028 0.67% 0.127% 14 23.422 1751 1756 1761 rBV 57483 114236 0.99% 0.186% 15 24.849 1877 1881 1889 rVB 60981 110048 0.95% 0.180%

16 26.208 1997 2000 2007 rBV 37901 79416 0.69% 0.130% 17 26.835 2051 2055 2061 rVB 34181 73408 0.63% 0.120% 18 27.726 2129 2133 2139 rBV 922420 1654704 14.30% 2.701% 19 30.489 2369 2375 2381 rBV 4394067 11022183 95.23% 17.994% 20 34.416 2713 2719 2749 rBV 3463331 9017817 77.91% 14.722%

Sum of corrected areas: 61255620

00557.D SCAN508.M Wed Jan 16 08:13:56 2002 Page 1

NYC-WTC_000051772

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NYC-WTC_000051772Source: NYC Law Department, mirrored locally

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