GCMS analysis results for sample AE00558, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00558.D Vial: 2 Acq On : 15 Jan 2002 2:21 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.602 17 20 23 rBV2 14141 25358 0.27% 0.049% 2 3.750 23 33 35 rBV4 5749 22839 0.24% 0.045% 3 4.858 123 130 139 rBV5 11313 41913 0.45% 0.082% 4 5.006 139 143 14 9 rW4 8994 21672 0.23% 0.042% 5 5.897 217 221 227 rBV 349693 892777 9.52% 1.742%

6 9.710 551 555 563 rW 2429263 5509233 58.77% 10.748% 7 9.858 563 568 575 rW 8240 30554 0.33% 0.060% 8 10.498 619 624 637 rBV4 8243 41501 0.44% 0.081% 9 12.541 799 803 809 rVB 13378 21760 0.23% 0.042% 10 13.192 855 860 865 rBV 4104920 7839104 83.62% 15.293%

11 13.295 865 869 875 rVB2 16109 35996 0.38% 0.070% 12 18.341 1305 1311 1315 rBV 4506863 8627366 92.03% 16.831% 13 22.280 1653 1656 1661 rBV 31916 59267 0.63% 0.116% 14 22.634 1681 1687 1693 rBV2 4397827 9374125 100.00% 18.288% 15 22.771 1695 1699 1713 rVB 47904 146022 1.56% 0.285%

16 24.849 1877 1881 1889 rW 17922 38178 0.41% 0.074% 17 27.726 2129 2133 2139 rW 728818 1285487 13.71% 2.508% 18 30.489 2369 2375 2381 rBV2 3976614 9244578 98.62% 18.035% 19 31.105 2421 2429 2449 rBV 66855 279477 2.98% 0.545% 20 34.416 2713 2719 2751 rBV 3043132 7720721 82.36% 15.062%

Sum of corrected areas: 51257928

00558.D SCAN508.M Wed Jan 16 08:14:00 2002 Page 1

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