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GCMS results for sample AE00560, Jan 17 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00560 showing surrogate recovery and unknown compounds detected on January 17, 2002.

NYC-WTC_000051740–000051754

Folder label: “GCMS X 1/9/02 A 1/15/02

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NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\02JAN15\00560.D Vial: 4 Acq On : 15 Jan 2002 4:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508 .M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.488 7 10 15 rVB 17109 24748 0.23% 0.044% 2 3.613 17 21 25 rVB 20772 37339 0.35% 0.066% 3 4.630 103 110 119 rVB4 12057 36406 0.34% 0.064% 4 4.846 125 129 141 rW5 12126 40191 0.38% 0.071% 5 5.018 141 144 14 9 rW2 13150 24261 0.23% 0.043% 6 5.897 217 221 229 rBV 437298 1041060 9.78% 1.843% 7 9.550 537 541 547 rBV 16937 44039 0.41% 0.078% 8 9.642 547 549 551 rW 15363 35027 0.33% 0.062% 9 9.710 551 555 561 rW 3130631 6147186 57.72% 10.883% 10 9.836 561 566 577 rVB 22762 70889 0.67% 0.126% 11 13.192 855 860 865 rBV 4727834 8808548 82.71% 15.595% 12 18.341 1305 1311 1315 rBV 4959231 9675784 90.86% 17.131% 13 22.280 1651 1656 1661 rVB2 35414 72702 0.68% 0.129% 14 22.645 1681 1688 1693 rBV2 4635641 10649308 100.00% 18.854% 15 22.771 1695 1699 1719 rVB 59025 174303 1.64% 0.309%

16 24.849 1877 1881 1887 rVB 29460 52407 0.49% 0.093% 17 27.726 2127 2133 2139 rBV 737416 1318968 12.39% 2.335% 18 30.489 2369 2375 2381 rBV2 4120018 10064948 94.51% 17.820% 19 31.105 2423 2429 2439 rVB3 17960 56428 0.53% 0.100% 20 34.416 2713 2719 2757 rBV 3150360 8107821 76.13% 14.355%

Sum of corrected areas: 56482363

0560.D SCAN508.M Wed Jan 16 08:14:08 2002 Page 1

NYC-WTC_000051744

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NYC-WTC_000051744Source: NYC Law Department, mirrored locally

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