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GCMS analysis results for sample AE00559, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00559 conducted on January 17, 2002.

NYC-WTC_000051727–000051739

Folder label: “GCMS X 1/9/02 A 1/15/02

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Scanned page image, NYC-WTC_000051731
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00559.D Vial: 3 Acq On : 15 Jan 2002 3:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.476 7 9 17 rVB 34934 54450 0.52% 0.094% 2 3.602 17 20 25 rBV 26635 40511 0.38% 0.070% 3 4.835 125 128 135 rBV2 23304 60803 0.58% 0.105% 4 5.885 217 220 227 rBV 685925 1315738 12.45% 2.267% 5 9.710 551 555 561 rW 3026749 6172834 58.42% 10.634%

6 9.847 561 567 577 rVB2 18500 55695 0.53% 0.096% 7 13.192 855 860 865 rBV 4690513 8878084 84.02% 15.294% 8 18.341 1305 1311 1315 rBV 4987877 9700869 91.81% 16.712% 9 19.997 1451 1456 1459 rBV2 25580 46044 0.44% 0.079% 10 22.280 1651 1656 1661 rVB 36729 69917 0.66% 0.120%

11 22.634 1681 1687 1693 rBV2 4744687 10566354 100.00% 18.203% 12 22.771 1695 1699 1711 rVB2 53567 159219 1.51% 0.274% 13 23.422 1751 1756 1763 rVB 22957 51056 0.48% 0.088% 14 24.849 1877 1881 1887 rBV 79209 138619 1.31% 0.239% 15 26.219 1995 2001 2007 rVB 18990 40038 0.38% 0.069%

16 26.847 2051 2056 2061 rVB 21088 45404 0.43% 0.078% 17 27.726 2127 2133 2139 rBV 857174 1527773 14.46% 2.632% 18 30.489 2369 2375 2381 rBV2 4304838 10387375 98.31% 17.895% 19 31.105 2425 2429 2447 rVB 34752 137465 1.30% 0.237% 20 34.416 2713 2719 2759 rBV 3331328 8599576 81.39% 14.815%

Sum of corrected areas: 58047824

00559.D SCAN508.M Wed Jan 16 08:14:04 2002 Page 1

NYC-WTC_000051731

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NYC-WTC_000051731Source: NYC Law Department, mirrored locally

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