GCMS analysis results for sample AE00556, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00556.D Vial: 3 . Acq On : 29 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 19 20 25 rBV 27003 50371 0.34% 0.063% 2 4.241 71 76 79 rBV3 18802 38623 0.26% 0.048% 3 4.630 103 110 119 rVB4 17082 52549 0.35% 0.066% 4 4.847 123 129 141 rBV3 26142 91131 0.61% 0.114% 5 5.885 217 220 247 rVB 688160 1637769 11.01% 2.054%

6 9.550 539 541 547 rBV3 17615 42294 0.28% 0.053% 7 9.710 551 555 561 rW 4193021 8497226 57.10% 10.658% 8 9.847 561 567 577 rVB 20975 60070 0.40% 0.075% 9 11.651 721 725 731 rW 49767 84542 0.57% 0.106% 10 12.542 799 803 807 rW 37291 62869 0.42% 0.079%

11 13.192 855 860 865 rBV 6324041 12044613 80.94% 15.108% 12 18.341 1305 1311 1315 rBV 6821914. 13372236 89.86% 16.773% 13 22.280 1651 1656 1661 rW 59920 109750 0.74% 0.138% 14 22.634 1681 1687 1693 rBV2 6447133 14881799 100.00% 18.667% 15 22.771 1695 1699 1713 rVB 81222 275019 1.85% 0.345%

16 24.849 1877 1881 1887 rBV 113561 204092 1.37% 0.256% 17 27.726 2129 2133 2137 rBV 1037072 1891314 12.71% 2.372% 18 30.489 2369 2375 2381 rBV2 5796383 14333883 96.32% 17.979% 19 31.105 2423 2429 2439 rW2 35688 134237 0.90% 0.168% 20 34.416 2713 2719 2747 rBV 4476065 11860239 79.70% 14.877%

Sum of corrected areas: 79724626

)0556.D SCAN508.M Wed Jan 30 09:01:56 2002 Page 1

NYC-WTC_000051553