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GCMS results for sample AE00561, Jan 17 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00561 showing surrogate recovery and unknown compounds detected on January 17, 2002.

NYC-WTC_000051755–000051767

Folder label: “GCMS X 1/9/02 A 1/15/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00561.D Vial: 5 Acq On : 15 Jan 2002 4 :50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508 .M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.488 7 10 19 rBV 25719 48707 0.46% 0.087% 2 3.602 19 20 25 rVB 19479 33780 0.32% 0.061% 3 4.630 107 110 119 rVB2 7981 21613 0.21% 0.039% 4 4.846 125 129 141 rVB5 15920 46087 0.44% 0.083% 5 5.897 217 221 229 rBV 417549 1004316 9.54% 1.801%

6 9.562 537 542 54 7 rW2 8729 24865 0.24% 0.045% 7 9.710 551 555 561 rW 3140570 6276984 59.63% 11.257% 8 9.847 561 567 577 rVB 14781 41592 0.40% 0.075% 9 12.541 799 803 807 rVB 13978 25996 0.25% 0.047% 10 13.192 855 860 865 rBV 4872073 8956446 85.08% 16.062%

11 13.375 873 876 887 rVB2 8829 23611 0.22% 0.042% 12 18.341 1305 1311 1315 rBV 4950973 9649122 91.66% 17.304% 13 19.997 1451 1456 1459 rBB2 14441 28704 0.27% 0.051% 14 22.280 1651 1656 1661 rBV2 33459 66653 0.63% 0.120% 15 22.645 1681 1688 1693 rBV2 4671976 10527160 100.00% 18.879%

16 22.771 1695 1699 1711 rVB 58137 173456 1.65% 0.311% 17 24.849 1877 1881 1887 rBV 84504 158319 1.50% 0.284% 18 27.726 2129 2133 2139 rW 660162 1129755 10.73% 2.026% 19 30.489 2369 2375 2381 rBV2 4122746 9727079 92.40% 17.444% 20 34.416 2713 2719 2749 rBV 3037568 7798012 74.08% 13.984%

Sum of corrected areas: 55762257

30561.D SCAN508.M Wed Jan 16 08:14:13 2002 Page 1

NYC-WTC_000051759

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NYC-WTC_000051759Source: NYC Law Department, mirrored locally

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