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GCMS analysis results for sample AE00106, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00106 analyzed on February 7, 2002.

NYC-WTC_000050774–000050792

Folder label: “GCMS X 1/4/02 A 1/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2JAN25\00106.D Vial: 5 Acq On : 25 Jan 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rBV 29725 50856 0.35% 0.064% 2 4.241 71 76 83 rW3 42289 87635 0.60% 0.110% 3 4.367 83 87 91 rVB3 16639 36636 0.25% 0.046% 4 4.629 107 110 117 rVB3 19126 43655 0.30% 0.055% 5 4.835 123 128 141 rBV3 33516 88598 0.61% 0.112%

6 5.885 217 220 243 rBV 649470 1489126 10.21% 1.874% 7 9.550 537 541 547 rBV3 12112 32446 0.22% 0.041% 8 9.710 551 555 563 rVB 4404223 8915759 61.15% 11.222% 9 9.847 563 567 573 rBV 18743 50822 0.35% 0.064% 10 12.541 799 803 811 rVB 25876 44730 0.31% 0.056%

11 13.192 855 860 865 rBV 6511424 12579349 86.27% 15.833% 12 13.375 873 876 883 rVB2 14373 31979 0.22% 0.040% 13 18.341 1305 1311 1315 rBV 6758882 13477411 92.43% 16.963% 14 22.280 1651 1656 1661 rVB 59491 114694 0.79% 0.144% 15 22.645 1681 1688 1693 rBV2 6382840 14581203 100.00% 18.353%

16 22.771 1697 1699 1717 rVB 88460 223435 1.53% 0.281% 17 27.726 2129 2133 2139 rW 1005721 1806287 12.39% 2.273% 18 30.500 2369 2376 2381 rBV 5753710 14007326 96.06% 17.630% 19 31.105 2419 2429 2437 rBV7 13959 57691 0.40% 0.073% 20 34.416 2713 2719 2749 rBV 4262981 11730304 80.45% 14.764%

Sum of corrected areas: 79449942

30106.D SCAN508.M Mon Jan 28 09:49:52 2002 Page 1

NYC-WTC_000050778

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NYC-WTC_000050778Source: NYC Law Department, mirrored locally

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