GCMS blank analysis results for sample AE00167, Jan 2002

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Data File : C:\MSDCHEM\1\5973N\O2JAN24\0104B.D Vial: 1 Acq On : 24 Jan 2002 11:41 am Operator: Sample : lab blankl/4 Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2-Methoxy-3-hydrazinyl-pyra... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.04 ug/L 19257 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW Mol Form CAS# Qual

1 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N4O 2 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 000000-00-0 74 001004-74-6 64 JO 3 2-Fluoronicotinamide 140 C6H5FN20 4 4(1H)-Pyrimidinone, 2-amino-6-(m... 140 C5H8N40 000364-22-7 39 054004-20-5 9 w(o Abundance Scan 876 (13.375 min): 0104B.D (-) m/z 140.00 100.00% 140

5000

70 94 49 —4 41,,................. —1 II 13.00 13.20 13.40 13.60 13.80 m/z 70.00 17.06% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35089: 2-Methoxy-3-hydrazinyl-pyrazine 140

5000 42 ■ । 1 1 1 1 r1 1 1 1 I ' ■ ‘ 1 i • 13.00 13.20 13.40 13.60 13.80 54 68 m/z 94.10 12.99% | 80 95 108 121 --------------------- • • i ‘ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 1-0 - 13.00 13.20 13.40 13.60 13.80 5000 m/z 141.10 9.87%

44 71 123 III 86 96 112 I H-.nl I. ■ I ' ' ' ‘ I ‘ ' ‘ । । | ‘ । , . --- i ■ ■ ' ■ i /z—> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35138:2-Fluoronicotinamide • i > - * ■ i • ■ -n-j-r-r-n-j-r 124 1-0 13.00 13.20 13.40 13.60 13.80 m/Z96.10 9.46% 96 5000 44 51 70 76

miz-> 30 40 50 mjl 60 70 80 ’14118 184 90 307 । । > । । । । । । i j_________ 100 110 120 1 1 i ■ ■ 130 140 —1, TII 13.00 13.20 13.40 13.60 13.80

)104B.D SCAN508.M Fri Jan 25 10:26:29 2002 Page 10

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