GCMS results for sample AE09092, April 30, 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\APR2502\9092 .D Vial: 23 Acq On : 26 Apr 2002 1:42 pm Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Hexadecanamide Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 32.23 1.10 ug/1 118484 Chrysene-dl2 33.64 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Hexadecanamide 255 C16H33NO 000629-54-9 78 2 9-Octadecenamide, (Z) - 281 C18H35NO 000301-02-0 56 3 Dodecanamide 199 C12H25NO 001120-16-7 45 4 Heptanamide, 4-ethyl-5-methyl- 171 C10H21NO 054789-40-1 39 Abundance 7 Scan 2961 (32.226 min): 9092.D (-) m/z 59.05 100.00% 69

5000 72 43 Tu ' ■ 31.80 32.00 32.20 32.40 32.60 86 98 114 128 142 156 170 184 240 254 283 m/z 72.00 42.57% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #34960: Hexadecanamide 59

5000 72 31,80 32.00 32.20 32.40 32.60 m/z 43.05 21.45% 86 100 114 128 ■ i ■ ■ ■ ■ r ■ • • ■: ■ ■’ ■ ■ । ■ ■ ■ ■ । * 170• । ■ ■ *198 212 226■ • । •' 255 ''i ■11 ■ । ■ ’■! ■ ■ ■ ■ । •.

mfz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72284:9-Octadecenamide, (Z)- 59

3180 3200 3220 3240 3260 ‘ 5000 72 m/ z 41.05 18.62% 44 | . 9 110122 136 ■ ■ i - ,22 mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 / Wk Abundance 59 #22660: Dodecanamide i ■ ■ ■ ■ i ■ ■ —A 31.80 32.00 32.20 32.40 32.60 m/z 55.00 14.54% 5000 72 44 86 100 114 128 156 170 199 I w THnp TDTT ' omAAg n/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 31.80 32.00 32.20 32.40 32.60

9092.D GCMS0412.M Fri Apr 26 14:50:25 2002 Page 4

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