GCMS results for sample AE09092, April 30, 2002

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Laboratory report documenting GCMS analysis of sample AE09092 conducted on April 30, 2002.

NYC-WTC_000049493–000049507

Folder label: “GCMS X 4/16/02 A 4/26/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\APR2502\9092.D Vial: 23 Acq On : 26 Apr 2002 1:42 pm Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *********************************** * ********************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 14.81 0.89 ug/1 120424 Naphthalene-d8 15.85 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxne, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Benzoic acid, /2,4-bis (trimethylsil 370 C16H3004Si3 010586-16-0—37 3 Benzeneethanamine, N- “ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 32 4 Benzoic acid, 2,6-bis (trimethylsil 370 C16H30O4Si3 003782-85-2 28 Abundance Scan 1064 (14.811 min): 9092.D (-) m/z 73.00 100.00% 73

5000 267 355

......... . 45 14.40 14.60 14.80 15.00 15.20 — 108 154 193 223 323 m/z 355.05 1’ 1***8 *r >■ j • f i —1 11/2//—//— 49.16% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 ................................ 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.00 47.87% .. |, , 323 | miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy}, trimet 73 ) 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 17.85% 45

......................................................................... .......................................... .. mfe—> 50 100 150 200 250 300 350 400 450 500 550 .......... ................................. Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 14.40 14.60 14.80 15.00 15.20 m/z 268.00 12.73% 5000

45 208 251 281 386 458 548 4 ' i ■ ‘ 1 ' i • ■ • ■ t ■ • ■ i ■ ■ ' ■ f ■ ■ ■ ■ i • ■ ■ ■ n ’ 11111’* miz—> 50 100 150 2tX) 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

9092.D GCMS0412.M Fri Apr 26 14:50:25 2002 Page 3

NYC-WTC_000049505

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NYC-WTC_000049505Source: NYC Law Department, mirrored locally

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