NYC-WTC_000046434
Laboratory report documenting GCMS analysis of sample AE09156 conducted on May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 11 pages
GCMS analysis results for sample AE09157, May 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AE09157 conducted on May 8, 2002.
NYC-WTC_000046445–000046455Folder label: “GCMS X 4/17/02 A 4/24 - 4/26/02”
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NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\1\DATA\APR2 502\9157.D Vial: 27 Acq On : 26 Apr 2002 6:30 pm Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
14.81 0.34 ug/1 46459 Naphthalene-d8 15.85
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 000541-02-6 90 370 C10H3005Si5 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 52 3 N-(Trifluproacetyl)-N,O,O',01 1 -tetr 553 C22H42F3NO4Si4 000000-00-0 43 4 Benzenee anamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 Abundance Scan 1064 (14.810 min): 9157.D (-) m/z 73.00 100.00% 73
267 355 5000 / TIB 45 14.40 14.60 14.80 15.00 15.20 154 193 223 ■ 11 ' 1 T T T —T + 1Tr 1 m/z 355.05 51.07% m/z->______50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 T-rT-r-r-j-r-r- 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.00 47.69% 207 323 ‘ U —IPP—mPPmmm — 1 I ' 1 1 ' I T T-r-T-[-r-r-r-r-J-r m/z-> 50 100 150 200 250 300350 400 450 500 550 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 ...................... / t.................. 14.40 14.60 14.80 15.00 15.20 267 m/z 356.05 17.74% 5000 179 356 45 147 I ' 1 i ' TTT 1 209 237 TT*TTI - 312 ,.................. m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-fTrifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi 73 14.40 14.60 14.80 15.00 15.20 m/z 268.00 13.06% 355 5000
45 Hrhr T 147 T———T ■ 193 267 ' TTTTTT I1. M ! |, , , , | ' TTI 538 ■ 1 i ' ' T 1 ' 1 ' I ' 1 1 1 I ' ' ' 1 I ' ' ' ' I ' ' m/z--> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
9157 .D GCMS0412.M Fri May 03 11:19:47 2002 Page 3
NYC-WTC_000046454
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NYC-WTC_000046454Source: NYC Law Department, mirrored locally
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