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GCMS results for sample AE09094, April 30, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09094 conducted on April 30, 2002.

NYC-WTC_000049508–000049517

Folder label: “GCMS X 4/16/02 A 4/26/02

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Scanned page image, NYC-WTC_000049516
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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\APR2502\9094 .D Vial: 25 Acq On : 26 Apr 2002 4:36 pm Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.81 0.63 ug/1 99553 Naphthalene-d8 15.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 3 Phenethylamine, N-methyl-.beta., 3,4 399 C18H37NO3Si3 010538-85-9 37 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 Abundance Scan 1063 (14.807 min): 9094.D (-) m/z 72.95 100.00% 73

5000 267 355 / \ 45 14.40 14.60 14.80 15.00 15.20 133154 193 223 1 323 i T i ■ ■ “L । । 'i THmptTTTgmmnuuu m/z 267.00 42.84% mfz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 39.51% 207 323 , | .. M I||1......... 1.... 1| .. ।.... ।.... |'..... .T|.... ।.... ।.... ।.... (... miz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #57357: Noradrenaline, tetra-TMS 73 T 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 14.76% 102

45 1 h ।..... ।TmaBMmpm 147 442 ..।...... । ... miz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #74239: Phenethylamine, N-methyl-.beta.13,4-tris(trimethyls i ■ 1 • 1 I 1 ' 1 ■ i ■ • ■ ‘ i ■ ■ ■ ■ i ■ ■ 73 14.40 14.60 14.80 15.00 15.20 m/z 357.05 10.80% 5000 355 44

m/z—> l 147 193 TWTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT 267 294 40 60 80 100 120 140160 180200220240260280300320 340360380 400 420440 ।1 ■ ■ ■ । ■' ■ ■ । 14.40 14.60 14.80 15.00 15.20

9094.D GCMS0412.M Mon Apr 29 11:14:27 2002 Page 2

NYC-WTC_000049516

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NYC-WTC_000049516Source: NYC Law Department, mirrored locally

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