GCMS analysis results for sample AE09156, May 2002

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Laboratory report documenting GCMS analysis of sample AE09156 conducted on May 8, 2002.

NYC-WTC_000046434–000046444

Folder label: “GCMS X 4/17/02 A 4/24 - 4/26/02”

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NYC 9/11 Public Portal Document

Data File : C : \HPCHEM\ 1 \DATA\ APR2 5029156.D Vial: 26 Acq On : 26 Apr 2002 5:32 pm Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 14.81 2.39 ug/1 335789 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual L______________ 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 32 Abundance l ' Scan 1063 (14.807 min): 9156.D (-) m/ z 73.00 100.00% 73

5000 267 355

ITT , i/ [ . ......... . I I . , "IT ‘ 45 14.40 14.60 14.80 15.00 15.20 108 133154 193 223 293 323 " ।I i । TTTmgTmtn TT TCTuupr m/z 355.05 43.83% m/z— Abundance 40 60 80 100120140160180 200 220 240 260280 300 320 340 360380 400420440 #51266: Cyclopentasiloxane, decamethyl- J 73

355 267 ... ..... ......... 5000 14,40 14.60 14.80 15.00 15.20 m/z 267.00 43.33% . ........................................ 207............. 323 i" " i ■ i ■" ■ ।" i ■ ■" i" " i1 ■ ■■ i'" ■ i" " i1' " i1"' i TTTTETTTTTTTTTWWIWTTTTTUT m/z-> 40 60 80 100120140160180 200220 240 260280 300320 340 360380400420440 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 .......... _ 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 15.96% 44

A.y. — TITTTm 147 193 267 294 I‘ ‘II‘‘‘I‘‘IAA‘‘‘L‘SI‘IVBIUOBUE‘B m/z-> _ 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #57357: Noradrenaline, tetra-TMS . , , , 73 14,40 14.60 14.80 15.00 15.20 m/ z 2 68.00 11.17%

5000 102 355

45 147 I Jf rri | u |-| | , i i i p ! ! , । i 442 ------- I" ’ 17 l'" 1 r " ■ i" " i" " r "11" " i' ■'1 r "11 i" " r "' r "11 ■" n/z—> 40 60 80 100120140160180200220240260280300320340360380400420440 14.40 14.60 14.80 15.00 15.20

9156.D GCMS0412.M Fri May 03 11:18:35 2002 Page 3

NYC-WTC_000046443

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GCMS analysis results for sample AE09157, May 2002 · Box DEP Box 27

NYC-WTC_000046445

Laboratory report documenting GCMS analysis of sample AE09157 conducted on May 8, 2002.

1 shared topics · Same agency, volume and box · similarity 0.998