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GCMS calibration data for sample AE08971, April 2002

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Calibration report detailing response factors for multiple analytes used in the analysis of sample AE08971.

NYC-WTC_000049405–000049411

Folder label: “GCMS X 4/16/02 A 4/26/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\APR25O2\CAL5O.D Vial: 2 Acq On 25 Apr 2002 9:33 am Operator: Sample Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 25 14:19 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table 1 Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412 1

Compound R.T. Qlon Response Cone Unit ) Qvalue 33) Hexachlorobenzene 24.69 284 469279 53.62 ug/1 95 34) Phenant hrene 25.66 178 1973630 50.15 ug/1 100 35) Anthrac ene 25.80 178 1951505 50.41 ug/1 100 36) Di-n-butylphthalate 27.56 149 2378068 48.30 ug/1 99 3 7) Fluoranthene 29.29 202 2006827 50.69 ug/1 95 4 0) Pyrene 29.96 202 2027298 46.84 ug/1 99 41) Butylbenzylphthalate 32.09 149 919135 43.43 ug/1 99 4 2) Benzo(a)anthracene 33.59 228 1499628 49.95 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 1151622 42.52 ug/1 99 44) Chrysene 33.73 228 1476384 49.59 ug/1 99 46) Di-n-Octylphthalate 35.60 149 1740179 41.45 ug/1 100 47) Benzo(b)fluoranthene 36.71 252 1256073 46.31 ug/1 98 4 8) Benzo(k)fluoranthene 36.78 252 1415554 53.59 ug/1 98 4 9) Benzo(a)pyrene 37.69 252 1131412 50.59 ug/1 99 50) Indeno (1,2,3-cd)pyrene 41.97 276 1084132 48.15 ug/1 97 51) Dibenz(a,h)anthracene 42.05 278 841326m 49.00 ug/1 52) Benzo(g,h,i)perylene 43.21 276 844463 44.93 ug/1 98

(#) = qualifier out of range (m) = manual integration CAL50.D GCMS0412.M Fri Apr 26 09:27:58 2002 1 Page 2

NYC-WTC_000049407

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NYC-WTC_000049407Source: NYC Law Department, mirrored locally

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