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GCMS calibration data for sample AE07484, May 2002

Machine-extracted title · confidence 90%

Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.

NYC-WTC_000044253–000044256

Folder label: “GCMS X 4/23/02 A 4/26/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR2 5 02\CAL50A.D Vial: 2 Acq On 26 Apr 2002 10:53 am Operator : Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 26 12:38 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Apr 25 15:21:43 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.70 284 761476 54.56 ug/1 95 34) Phenanthrene 25.67 178 3125824 49.81 ug/1 100 35) Anthracene 25.81 178 3096973 50.17 ug/1 100 36) Di-n-butylphthalate 27.57 149 3809247 48.52 ug/1 100 37) Fluoranthene 29.30 202 3182283 50.41 ug/1 # 92 4 0) Pyrene 29.97 202 3199694 47.86 ug/1 97 41) Butylbenzylphthalate 32.09 149 1464786 44.80 ug/1 99 42) Benzo(a)anthracene 33.60 228 2340963 50.48 ug/1 100 43) Bis(2-ethylhexyl)phthalate 33.87 149 1796495 42.94 ug/1 # 99 44) Chrysene 33.74 228 2261520 49.17 ug/1 99 46) Di-n-Octylphthalate 35.62 149 2692403 43.17 ug/1 # 98 47) Benzo(b)fluoranthene 36.72 252 1935230 48.03 ug/1 98 48) Benzo(k)fluoranthene 36.79 252 2065022 52.63 ug/1 97 4 9) Benzo(a)pyrene 37.70 252 1673585 50.38 ug/1 99 50) Indeno(1,2,3-cd)pyrene 42.00 276 1591066m 47.57 ug/1 51) Dibenz(a,h)anthracene 42.06 278 1233379 48.36 ug/1 96 52) Benzo(g,h,i)perylene 43.24 276 1246909 44.66 ug/1 96

(#) = qualifier out of range (m) = manual integration CAL50A.D GCMS0501.M Wed May 01 11:18:25 2002 Page 2

NYC-WTC_000044255

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NYC-WTC_000044255Source: NYC Law Department, mirrored locally

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