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GCMS analysis results for sample AE08486, May 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE08486 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000048647–000048659

Folder label: “GCMS X 4/10/02 A 4/20/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\DATA\020419\08484.D Vial: 21 Acq On : 20 Apr 2002 3:49 am Operator: Nefliu Sample : sample . Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.355 36 47 53 W 2 19705 341975 0.37% 0.066% 2 3.655 94 98 106 W 2 26173 384407 0.41% 0.074% 3 3.743 106 113 116 PV 2 5645 92502 0.10% 0.018% 4 5.171 352 356 362 PV 6 7593 146196 0.16% 0.028% 5 6.158 510 524 565 PV 922300 18727825 20.00% 3.591% 6 6.410 565 567 579 W 6 5505 137524 0.15% 0.026% 7 11.375 1399 1412 1430 PV 2396358 59345378 63.39% 11.380% 8 14.407 1916 1928 1935 PV 4 6673 171137 0.18% 0.033% 9 16.534 2270 2290 2310 PV 2979466 82247270 87.85% 15.771% 10 16.757 2323 2328 2338 W 2 11625 269881 0.29% 0.052% 11 17.409 2433 2439 2449 PV 4 7123 152023 0.16% 0.029% 12 24.460 3620 3639 3657 PV 3198461 93619202 100.00% 17.952% 13 27.539 4143 4163 4173 PV 3 332150 9568087 10.22% 1.835% 14 31.088 4751 4767 4778 W 2 23213 767990 0.82% 0.147% 15 31.722 4855 4875 4892 W 2 2989441 93328443 99.69% 17.896% 16 31.957 4902 4915 4931 W 2 29272 930552 0.99% 0.178% 17 34.807 5383 5400 5406 PV 2 7085 214286 0.23% 0.041% 18 39.225 6147 6152 6156 W 3 13412 261880 0.28% 0.050% 19 39.936 6259 6273 6299 PV 2 4206305 85488375 91.32% 16.393% 20 40.436 6351 6358 6366 W 3 18284 434653 0.46% 0.083% 21 40.530 6366 6374 6382 W 2 7128 219555 0.23% 0.042% 22 43.162 6808 6822 6849 PV 2 3539110 74656033 79.74% 14.315%

Sum of corrected areas: 521505172

08484.D SCAN020418.M Thu May 02 11:45:21 2002 Page 1

NYC-WTC_000048652

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NYC-WTC_000048652Source: NYC Law Department, mirrored locally

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