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GCMS sample analysis report AE08483, May 7 2002

Machine-extracted title · confidence 95%

Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.

NYC-WTC_000048623–000048634

Folder label: “GCMS X 4/10/02 A 4/20/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\1\DATA\020419\08482.D Vial: 19 Acq On : 20 Apr 2002 1:51 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.361 45 48 51 W 2 23359 250586 0.29% 0.053% 2 3.661 82 99 110 PV 2 20054 385496 0.44% 0.082% 3 4.307 201 209 220 PV 100028 1433223 1.65% 0.305% 4 5.171 354 356 360 W 4 6008 77924 0.09% 0.017% 5 6.158 515 524 563 PV 868528 17753146 20.48% 3.778% 6 11.375 1400 1412 1434 PV 2205883 55160088 63.62% 11.739% 7 16.534 2270 2290 2310 W 2899038 76670694 88.43% 16.317% 8 16.763 2316 2329 2340 PV 2 9851 328441 0.38% 0.070% 9 24.460 3622 3639 3658 PV 3089494 86705818 100.00% 18.453% 10 27.539 4142 4163 4174 PV 2 326234 9172605 10.58% 1.952% 11 31.088 4756 4767 4776 W 3 22996 736271 0.85% 0.157% 12 31.717 4857 4874 4895 W 2 2795850 85510809 98.62% 18.198% 13 31.952 4907 4914 4924 W 5 27245 733203 0.85% 0.156% 14 34.807 5392 5400 5406 PV 9805 199651 0.23% 0.042% 15 35.882 5577 5583 5591 W 3 13586 269754 0.31% 0.057% 16 39.226 6144 6152 6158 PV 4 9359 206204 0.24% 0.044% 17 39.931 6260 6272 6288 PV 2 3723013 72178479 83.25% 15.361% 18 40.031 6288 6289 6293 W 8784 124754 0.14% 0.027% 19 40.442 6349 6359 6367 W 4 13535 357694 0.41% 0.076% 20 40.530 6367 6374 6385 W 3 13531 394667 0.46% 0.084% 21 43.156 6807 6821 6839 PV 2 3001372 61232359 70.62% 13.031%

Sum of corrected areas: 469881864

08482.D SCAN020418.M Thu May 02 11:44:24 2002 Page 1

NYC-WTC_000048627

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NYC-WTC_000048627Source: NYC Law Department, mirrored locally

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