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GCMS analysis results for sample AE08431, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048121–000048133

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048125
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020419\08431.D Vial: 18 Acq On : 20 Apr 2002 12:52 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.126 3 8 17 BV 32069 357694 0.41% 0.078% 2 5.006 321 328 343 PV 2 33719 681179 0.77% 0.149% 3 5.799 459 463 473 W 2 22818 429712 0.49% 0.094% 4 6.128 514 519 53 0 PV 2 8158 247503 0.28% 0.054% 5 11.375 1398 1412 1435 PV 2176886 56683712 64.31% 12.390%

6 16.540 2275 2291 2309 PV 2994224 78461784 89.02% 17.150% 7 16.769 2316 2330 2339 W 10466 305567 0.35% 0.067% 8 24.466 3617 3640 3658 PV 3171048 88139227 100.00% 19.266% 9 27.539 4149 4163 4178 PV 2 277311 7627673 8.65% 1.667% 10 31.088 4757 '4767 4780 W 5 21575 755897 0.86% 0.165%

11 31.722 4855 4875 4893 W 2 2881072 86544954 98.19% 18.917% 12 31.957 4905 4915 4923 PV 3 28699 725655 0.82% 0.159% 13 34.813 5393 5401 5405 PV 2 8942 184453 0.21% 0.040% 14 39.226 6147 6152 6161 W 2 14983 307044 0.35% 0.067% 15 39.936 6260 6273 6292 W 2 3599549 72752281 82.54% 15.902%

16 40.436 6353 6358 6368 W 3 17706 408946 0.46% 0.089% 17 40.524 6368 6373 6380 W 2 12147 308507 0.35% 0.067% 18 43.156 6799 6821 6837 PV 3110967 62432601 70.83% 13.647% 19 43.262 6837 6839 6846 W 7252 137369 0.16% 0.030%

Sum of corrected areas: 457491759

08431.D SCAN020418 .M Thu May 02 15:40:21 2002 Page 1

NYC-WTC_000048125

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NYC-WTC_000048125Source: NYC Law Department, mirrored locally

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