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GCMS analysis results for sample AE08429, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08429 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048207–000048219

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048211
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020419\08429.D Vial: 16 Acq On : 19 Apr 2002 10:54 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.132 3 9 14 BV 4 21348 249477 0.29% 0.054% 2 5.006 321 328 336 W 3 63034 1108360 1.29% 0.242% 3 5.799 456 463 4 73 PV 2 42527 888412 1.03% 0.194% 4 6.111 512 516 535 PV 3 17923 528838 0.62% 0.115% 5 11.375 1397 1412 1441 PV 2095624 54544882 63.47% 11.904%

6 16.540 2276 2291 2306 PV 2967568 75761339 88.16% 16.535% 7 16.763 2321 2329 2340 W 2 8045 224370 0.26% 0.049% 8 24.460 3617 3639 3655 W 3077260 85931608 100.00% 18.754% 9 27.539 4149 4163 4179 PV 2 259419 7141468 8.31% 1.559% 10 31.088 4756 4767 4778 W 4 20754 630738 0.73% 0.138%

11 31.722 4855 4875 4888 PV 3 2823406 85361587 99.34% 18.630% 12 31.951 4908 4914 4922 W 2 24939 605214 0.70% 0.132% 13 34.807 5384 5400 5409 W 2 9854 287513 0.33% 0.063% 14 36.047 5604 5611 5619 PV 4 16012 348829 0.41% 0.076% 15 36.658 5706 5715 5726 PV 2 9227 200092 0.23% 0.044%

16 39.225 6139 6152 6161 W 3 11729 291959 0.34% 0.064% 17 39.936 6260 6273 6286 PV 2 3812534 77444568 90.12% 16.902% 18 40.048 6286 6292 6304 W 4 19934 754779 0.88% 0.165% 19 40.436 6353 6358 6365 PV 4 15952 331317 0.39% 0.072% 20 43.156 6809 6821 6841 PV 3275303 65557158 76.29% 14.308%

Sum of corrected areas: 458192508

08429.D SCAN020418.M Thu May 02 15:37:56 2002 Page 1

NYC-WTC_000048211

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NYC-WTC_000048211Source: NYC Law Department, mirrored locally

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