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GCMS analysis results for sample AE08323, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048106–000048120

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048110
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020419\08323.D Vial: 10 Acq On : 19 Apr 2002 4:59 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.126 3 8 18 BV 38584 402832 0.48% 0.087% 2 3.332 39 43 48 W 2 21057 332843 0.39% 0.072% 3 3.631 88 94 104 PV 3 18970 332647 0.39% 0.072% 4 6.117 511 517 53 0 PV 3 27696 720921 0.85% 0.157% 5 11.375 1399 1412 1433 BV 2079270 53813460 63.55% 11.684%

6 16.534 2270 2290 2312 PV 2864942 74761303 88.29% 16.232% 7 16.769 2323 2330 2338 W 2 10500 271749 0.32% 0.059% 8 24.460 3616 3639 3654 PV 3013917 84458135 99.74% 18.337% 9 27.539 4131 4163 4178 PV 2 257009 7163049 8.46% 1.555% 10 31.088 4758 4767 4777 W 4 20578 592748 0.70% 0.129%

11 31.722 4853 4875 4901 W 2 2769005 84677180 100.00% 18.384% 12 31.952 4906 4914 4925 W 4 25894 736473 0.87% 0.160% 13 34.807 5385 5400 5406 W 2 16285 371013 0.44% 0.081% 14 39.226 6146 6152 6172 W 4 13385 402682 0.48% 0.087% 15 39.937 6260 6273 6285 PV 2 3803541 78691918 92.93% 17.085%

16 40.013 6285 6286 6289 W 12091 137424 0.16% 0.030% 17 40.042 6289 6291 6311 W 4 13322 514833 0.61% 0.112% 18 40.436 6353 6358 6365 PV 2 18697 373238 0.44% 0.081% 19 40.530 6365 6374 6379 W 3 8532 214443 0.25% 0.047% 20 43.162 6809 6822 6843 PV 2 3435612 71419282 84.34% 15.506%

21 43.315 6843 6848 6859 W 2 6353 202905 0.24% 0.044%

Sum of corrected areas: 460591076

08323.D SCAN020418 ,M Thu May 02 15:23:46 2002 Page 1

NYC-WTC_000048110

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NYC-WTC_000048110Source: NYC Law Department, mirrored locally

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