GCMS analysis results sample AE08486, May 2002

NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\DATA\020419\08483.D Vial: 20 Acq On : 20 Apr 2002 2:50 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.355 43 47 53 PV 3 12720 148464 0.17% 0.031% 2 3.655 91 98 107 PV 2 16929 266454 0.31% 0.056% 3 5.171 353 356 362 W 3 7839 120266 0.14% 0.025% 4 6.128 512 519 520 PV 26998 362359 0.42% 0.076% 5 6.158 520 524 554 W 798426 16220868 19.01% 3.420% 6 6.340 554 555 562 W 5 16623 354282 0.42% 0.075% 7 11.375 1399 1412 1431 PV 2152238 54061377 63.36% 11.398% 8 16.534 2275 2290 2306 PV 2852364 75108403 88.03% 15.836% 9 16.769 2323 2330 2337 W 2 8463 203789 0.24% 0.043% 10 24.460 3618 3639 3655 BV 3047776 85322485 100.00% 17.989% 11 27.539 4146 4163 4187 PV 2 323679 9025070 10.58% 1.903% 12 31.094 4755 4768 4780 PV 3 20974 755726 0.89% 0.159% 13 31.722 4856 4875 4889 W 2 2780189 85131535 99.78% 17.949% 14 31.952 4901 4914 4922 W 3 26614 732285 0.86% 0.154% 15 34.807 5395 5400 5406 W 2 10846 212978 0.25% 0.045% 16 39.225 6143 6152 6158 PV 3 10969 245782 0.29% 0.052% 17 39.936 6258 6273 6287 W 2 3759935 78044040 91.47% 16.455% 18 40.025 6287 62'88 6304 W 4 9118 344631 0.40% 0.073% 19 40.436 6352 6358 6365 PV 2 15660 348692 0.41% 0.074% 20 40.530 6365 6374 6382 W 3 15332 421371 0.49% 0.089% 21 43.156 6809 6821 6841 PV 2 3224451 66864948 78.37% 14.098%

Sum of corrected areas: 474295805

08483.D SCAN020418.M Thu May 02 11:44:49 2002 Page 1

NYC-WTC_000048639