GCMS analysis results for sample AE08427, May 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020419\08427.D Vial: 14 Acq On : 19 Apr 2002 8:56 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.132 3 9 16 BV 2 14820 161508 0.18% 0.034% 2 5.012 323 329 339 PV 2 37198 686942 0.77% 0.144% 3 5.805 458 464 4 72 PV 3 23975 479810 0.54% 0.100% 4 6.117 506 517 529 W 2 15777 549792 0.61% 0.115% 5 11.375 1397 1412 1435 PV 2180254 56931102 63.59% 11.894%

6 16.540 2275 2291 2304 PV 3044551 78769234 87.98% 16.457% 7 16.769 2315 2330 2336 BV 2 8389 198213 0.22% 0.041% 8 24.466 3621 3640 3653 PV 3179536 89526414 100.00% 18.704% 9 27.539 4150 4163 4173 W 251489 7015488 7.84% 1.466% 10 31.094 4751 4768 4776 PV 4 23570 772249 0.86% 0.161%

11 31.723 4856 4875 4888 W 2 3010889 89382314 99.84% 18.674% 12 31.963 4903 4916 4924 PV 3 28866 806229 0.90% 0.168% 13 34.807 5392 5400 5411 PV 2 13513 306814 0.34% 0.064% 14 39.226 6145 6152 6166 PV 2 14375 322941 0.36% 0.067% 15 39.937 6260 6273 6289 W 2 3888513 81177342 90.67% 16.960%

16 40.042 6289 6291 6293 W 2 8524 104525 0.12% 0.022% 17 40.066 6293 6295 6300 W 9805 164027 0.18% 0.034% 18 40.442 6347 6359 6368 PV 22015 482083 0.54% 0.101% 19 40.530 6368 6374 6384 W 4 11131 267471 0.30% 0.056% 20 43.156 6810 6821 6847 PV 2 3389589 70412732 78.65% 14.711%

21 44.766 7089 7095 7101 PV 2 5311 123912 0.14% 0.026%

Sum of corrected areas: 478641143

08427.D SCAN020418.M Thu May 02 15:34:16 2002 Page 1

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