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GCMS analysis results for sample AE08324, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08324 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048134–000048147

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048138
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020419\08324 .D Vial: 11 Acq On : 19 Apr 2002 5:58 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.138 3 10 20 BV 2 35090 439218 0.50% 0.095% 2 3.338 41 44 51 W 2 28888 376356 0.43% 0.081% 3 3.637 89 95 105 PV 2 26365 433217 0.50% 0.094% 4 5.018 326 330 338 PV 5 6353 120185 0.14% 0.026% 5 5.159 349 354 368 W 4 8827 229500 0.26% 0.050%

6 5.811 461 465 468 PV 2 7224 87447 0.10% 0.019% 7 6.117 512 517 534 W 3 40187 1042937 1.19% 0.225% 8 11.375 1397 1412 1430 PV 2145768 56057876 64.05% 12.115% 9 16.540 2276 2291 2305 PV 2983885 77582747 88.65% 16.767% 10 16.763 2320 2329 2334 W 2 6943 120946 0.14% 0.026%

11 24.460 3620 3639 3650 PV 3235216 87517075 100.00% 18.914% 12 27.539 4149 4163 4175 PV 2 275166 7402014 8.46% 1.600% 13 31.094 4757 4768 4784 PV 5 20394 631290 0.72% 0.136% 14 31.723 4857 4875 4887 W 2 2925705 87054063 99.47% 18.814% 15 31.958 4903 4915 4932 W 4 26544 808745 0.92% 0.175%

16 34.807 5391 5400 5408 PV 2 17802 397715 0.45% 0.086% 17 39.226 6138 6152 6158 PV 3 13742 245099 0.28% 0.053% 18 39.937 6259 6273 6290 PV 2 3913064 76732322 87.68% 16.583% 19 40.048 6290 6292 6303 W 2 11276 340388 0.39% 0.074% 20 40.442 6349 6359 6368 PV 3 15835 397505 0.45% 0.086%

21 40.524 6368 6373 6382 W 3 14527 348175 0.40% 0.075% 22 43.156 6806 6821 6857 PV 2 3163529 64349448 73.53% 13.907%

Sum of corrected areas: 462714269

08324.D SCAN020418.M Fri May 03 09:04:29 2002 Page 1

NYC-WTC_000048138

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NYC-WTC_000048138Source: NYC Law Department, mirrored locally

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