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GCMS analysis results for sample AE08428, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08428 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048195–000048206

Folder label: “GCMS X 4/9/02 A 4/19/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020419\08428.D Vial: 15 Acq On : 19 Apr 2002 9:55 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0.01 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.144 5 11 21 BV 2 29939 385014 0.41% 0.078% 2 6.105 507 515 522 PV 2 18191 399027 0.43% 0.081% 3 6.152 522 523 540 W 4 8351 203670 0.22% 0.041% 4 11.375 1398 1412 1445 PV 2272732 59636628 63.86% 12.127% 5 16.540 2274 2291 2317 PV 3080774 82626641 88.48% 16.802%

6 16.763 2325 2329 2339 VB 9728 198615 0.21% 0.040% 7 24.460 3621 3639 3652 PV 3339730 93385092 100.00% 18.989% 8 27.539 4144 4163 4174 PV 2 268673 7330991 7.85% 1.491% 9 31.094 4757 4768 4778 W 4 22193 675994 0.72% 0.137% 10 31.722 4854 4875 4888 PV 2 3001029 92725591 99.29% 18.855%

11 31.957 4906 4915 4923 W 3 24983 641759 0.69% 0.130% 12 34.807 5392 5400 5407 PV 2 10351 215807 0.23% 0.044% 13 39.226 6147 6152 6158 PV 2 10504 199518 0.21% 0.041% 14 39.936 6260 6273 6289 BV 2 4150919 82644140 88.50% 16.805% 15 40.442 6346 6359 6367 PV 5 15394 416050 0.45% 0.085%

16 40.524 6367 6373 6378 W 2 10773 214050 0.23% 0.044% 17 43.156 6809 6821 6843 PV 2 3492732 69803534 74.75% 14.194% 18 43.303 6843 6846 6852 W 5341 75306 0.08% 0.015%

Sum of corrected areas: 491777427

08428.D SCAN020418.M Thu May 02 15:35:59 2002 Page 1

NYC-WTC_000048199

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NYC-WTC_000048199Source: NYC Law Department, mirrored locally

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